3-(2-o-methoxyphenylethylidene)isoindolinone

Base Information

Chemical Name:3-(2-o-methoxyphenylethylidene)isoindolinone
CAS No.:137406-48-5
Molecular Formula:C₁₇H₁₅NO₂
Molecular Weight:265.312
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-o-methoxyphenylethylidene)isoindolinone

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Technology Process of 3-(2-o-methoxyphenylethylidene)isoindolinone

There total 4 articles about 3-(2-o-methoxyphenylethylidene)isoindolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-Hydroxy-3-[2-(2-methoxy-phenyl)-ethyl]-2,3-dihydro-isoindol-1-one

: 137406-48-5
3-(2-o-methoxyphenylethylidene)isoindolinone

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; for 0.5h; Yield given; Ambient temperature;
DOI:10.1248/cpb.41.2003

Reference yield:

: 7417-18-7
2-methoxyphenethyl alcohol

: 137406-48-5
3-(2-o-methoxyphenylethylidene)isoindolinone

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / thionyl chloride / benzene / 2 h / 50 °C

2: 1.) Mg / 1.) THF, 50 deg C, 1 h, 2.) THF, RT, 8 h

3: 15percent aq. HCl / tetrahydrofuran / 0.5 h / Ambient temperature

With hydrogenchloride; thionyl chloride; magnesium; In tetrahydrofuran; benzene;
DOI:10.1248/cpb.41.2003

Reference yield:

: 93-25-4
2-methoxyphenylacetic acid

: 137406-48-5
3-(2-o-methoxyphenylethylidene)isoindolinone

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / lithium aluminum hydride / diethyl ether / 0.5 h / Heating

2: 75 percent / thionyl chloride / benzene / 2 h / 50 °C

3: 1.) Mg / 1.) THF, 50 deg C, 1 h, 2.) THF, RT, 8 h

4: 15percent aq. HCl / tetrahydrofuran / 0.5 h / Ambient temperature

With hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; magnesium; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1248/cpb.41.2003