RuH2(η2:η2-H2B(t)Bu)2(PCy3)2

Base Information

Chemical Name:RuH2(η2:η2-H2B(t)Bu)2(PCy3)2
CAS No.:1187559-68-7
Molecular Formula:C₄₀H₇₉BP₂Ru
Molecular Weight:733.896
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of RuH2(η2:η2-H2B(t)Bu)2(PCy3)2

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Technology Process of RuH2(η2:η2-H2B(t)Bu)2(PCy3)2

There total 1 articles about RuH2(η2:η2-H2B(t)Bu)2(PCy3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 75-77-4
chloro-trimethyl-silane

: 112320-11-3
RuH₂(H₂)2(tricyclohexylphosphine)2

: 124287-19-0
lithium isobutyltrihydroborate

: 1187559-68-7
RuH2(η2:η2-H2B(t)Bu)2(PCy3)2

Guidance literature:: In diethyl ether; toluene; byproducts: H2; (Ar); Me3SiCl was added to ethereal soln. of lithium tert-butylborohydride at room temp., stirred for 5 h, transfered to soln. of ruthenium complex in toluene, stirred for 5 h; evapd., pentane was added, filtered through celite, filtrate was evapd.;
DOI:10.1016/j.jorganchem.2009.03.020