Technology Process of 2-(4-dodecylbenzoyl)hydrazinecarboximidamide hydrochloride
There total 7 articles about 2-(4-dodecylbenzoyl)hydrazinecarboximidamide hydrochloride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 9-borabicyclo[3.3.1]nonane / tetrahydrofuran
1.2: 4 h / Reflux
2.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 1 h / 20 °C
3.1: acetyl chloride / methanol / 0.17 h / 0 °C / Reflux
4.1: hydrazine / ethanol / Reflux
5.1: N-ethyl-N,N-diisopropylamine / acetonitrile
6.1: trifluoroacetic acid / dichloromethane
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; 9-borabicyclo[3.3.1]nonane; N-ethyl-N,N-diisopropylamine; acetyl chloride; trifluoroacetic acid; hydrazine;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetonitrile; tert-butyl alcohol;
1.2: |Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine / acetonitrile
2: trifluoroacetic acid / dichloromethane
With
N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 9-borabicyclo[3.3.1]nonane / tetrahydrofuran
1.2: 4 h / Reflux
2.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 1 h / 20 °C
3.1: acetyl chloride / methanol / 0.17 h / 0 °C / Reflux
4.1: hydrazine / ethanol / Reflux
5.1: N-ethyl-N,N-diisopropylamine / acetonitrile
6.1: trifluoroacetic acid / dichloromethane
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; 9-borabicyclo[3.3.1]nonane; N-ethyl-N,N-diisopropylamine; acetyl chloride; trifluoroacetic acid; hydrazine;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetonitrile; tert-butyl alcohol;
1.2: |Suzuki Coupling;