(C₂₀H₈N₄(p-tolyl)4(CH₃))FeCl

Base Information

Chemical Name:(C₂₀H₈N₄(p-tolyl)4(CH₃))FeCl
CAS No.:95675-71-1
Molecular Formula:C₄₉H₃₉ClFeN₄
Molecular Weight:775.175
Hs Code.:

(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(p-tolyl)4(CH<sub>3</sub>))FeCl

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Chemical Property of (C₂₀H₈N₄(p-tolyl)4(CH₃))FeCl

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Technology Process of (C₂₀H₈N₄(p-tolyl)4(CH₃))FeCl

There total 1 articles about (C₂₀H₈N₄(p-tolyl)4(CH₃))FeCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N²¹-methyl-5,10,15,20-tetrakis(p-tolyl)porphyrin

: 7705-08-0
iron(III) chloride

: 7439-89-6
iron

: 95675-71-1,138661-31-1
(C₂₀H₈N₄(p-tolyl)4(CH₃))FeCl

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine; In tetrahydrofuran; dry O2-free THF was added to anhyd. FeCl3 and excess of Fe powder, heated under reflux in N2 for 2-3 h, THF soln. of N-alkylporphyrine was added, mixt. was removed from heat, 2,2,6,6-tetramethylpiperidine was added until soln. was slightly basic, 1 h; filtered through Celite, solvent removed, recrystd. from CH2Cl2-n-hexane;