3,5-DIFLUOROBENZYLZINC BROMIDE

Base Information

Chemical Name:3,5-DIFLUOROBENZYLZINC BROMIDE
CAS No.:308796-30-7
Molecular Formula:C₇H₅BrF₂Zn
Molecular Weight:272.408
Hs Code.:2827590000
Mol file:308796-30-7.mol

Synonyms:

Suppliers and Price of 3,5-DIFLUOROBENZYLZINC BROMIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
3,5-Difluorobenzylzinc bromide solution 0.5M in THF
50ml
$ 372.00

Rieke Metals
3,5-Difluorobenzylzincbromide
100mL
$ 700.00

Rieke Metals
3,5-Difluorobenzylzincbromide
50mL
$ 426.00

Rieke Metals
3,5-Difluorobenzylzincbromide
50mL
$ 426.00

American Custom Chemicals Corporation
3,5-DIFLUOROBENZYLZINC BROMIDE 95.00%
1L
$ 9471.00

American Custom Chemicals Corporation
3,5-DIFLUOROBENZYLZINC BROMIDE 95.00%
500ML
$ 6699.00

American Custom Chemicals Corporation
3,5-DIFLUOROBENZYLZINC BROMIDE 95.00%
100ML
$ 3049.20

Total 11 raw suppliers

Chemical Property of 3,5-DIFLUOROBENZYLZINC BROMIDE

Chemical Property:

Flash Point:1?°F
Density:0.982?g/mL?at 25?°C
Storage Temp.:2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

3,5-Difluorobenzylzinc bromide solution 0.5M in THF ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:F,Xn
Statements: 19-22-36/38-40-36/37-14-11
Safety Statements: 16-26-33-36-36/37

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,5-DIFLUOROBENZYLZINC BROMIDE

There total 1 articles about 3,5-DIFLUOROBENZYLZINC BROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 141776-91-2
1-bromomethyl-3,5-difluoro-benzene

: 7440-66-6
zinc

: 308796-30-7
bromo-[(3,5-difluorophenyl)methyl]zinc

Guidance literature:: In tetrahydrofuran; for 0.5h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2014.05.088

Reference yield: 75.0%

: 308796-30-7
bromo-[(3,5-difluorophenyl)methyl]zinc

: 914349-79-4
tert-butyl N-(5-bromopyrazin-2-yl)carbamate

: tert-butyl N-[5-[(3,5-difluorophenyl)methyl]pyrazin-2-yl]carbamate

Guidance literature:: tert-butyl N-(5-bromopyrazin-2-yl)carbamate; With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); In 1,4-dioxane; at 20 ℃; for 0.0833333h; Inert atmosphere;

bromo-[(3,5-difluorophenyl)methyl]zinc; In 1,4-dioxane; at 60 ℃; for 2h;

Reference yield:

: 308796-30-7
bromo-[(3,5-difluorophenyl)methyl]zinc

: 1458652-58-8
methyl 2-((S)-6-((R)-4-bromo-7-fluoro-2,3-dihydro-1H-inden-1-yloxy)-2,3-dihydrobenzofuran-3-yl)acetate

: 1471996-81-2
{(S)-6-[(R)-4-(3,5-difluoro-benzyl)-7-fluoro-indan-1-yloxy]-2,3-dihydro-benzofuran-3-yl}-acetic acid methyl ester

Guidance literature:: With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; In tetrahydrofuran; at 60 ℃; Inert atmosphere;