2,2-dibutyl-1,6,7,8-tetraaza-2-stannabicyclo[3.3.0]octa-5,7-diene

Base Information

Chemical Name:2,2-dibutyl-1,6,7,8-tetraaza-2-stannabicyclo[3.3.0]octa-5,7-diene
CAS No.:157843-29-3
Molecular Formula:C₁₁H₂₂N₄Sn
Molecular Weight:329.032
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-dibutyl-1,6,7,8-tetraaza-2-stannabicyclo[3.3.0]octa-5,7-diene

Chemical Property:

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Technology Process of 2,2-dibutyl-1,6,7,8-tetraaza-2-stannabicyclo[3.3.0]octa-5,7-diene

There total 2 articles about 2,2-dibutyl-1,6,7,8-tetraaza-2-stannabicyclo[3.3.0]octa-5,7-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 157843-28-2
5-[2-(dibutylphenylstannyl)ethyl]-2-(tributylstannyl)tetrazole

: 157843-29-3
2,2-dibutyl-1,6,7,8-tetraaza-2-stannabicyclo[3.3.0]octa-5,7-diene

: 960-16-7
tributylphenylstannane

Guidance literature:: In neat (no solvent); Sn-compd. is heated at 170°C for 12 h, cooling to room temp.; washing with light petroleum (b.p. 60-80°C), petroleum ether washings contain SnBu3Ph which is isolated by distn. under vac., residue isheated at 48°C under vac., elem. anal.;
DOI:10.1039/DT9940002135

Reference yield:

: 157843-38-4
dibutyl(2-cyanoethyl)phenylstannane

: 17846-68-3
azido tributyltin (IV)

: 157843-29-3
2,2-dibutyl-1,6,7,8-tetraaza-2-stannabicyclo[3.3.0]octa-5,7-diene

: 960-16-7
tributylphenylstannane

Guidance literature:: Multi-step reaction with 2 steps

1: neat (no solvent)

2: neat (no solvent)

In neat (no solvent);
DOI:10.1039/DT9940002135