dibutyl(2-cyanoethyl)phenylstannane

Base Information

Chemical Name:dibutyl(2-cyanoethyl)phenylstannane
CAS No.:157843-38-4
Molecular Formula:C₁₇H₂₇NSn
Molecular Weight:364.118
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibutyl(2-cyanoethyl)phenylstannane

Chemical Property:

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Technology Process of dibutyl(2-cyanoethyl)phenylstannane

There total 1 articles about dibutyl(2-cyanoethyl)phenylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 157843-37-3
phenyldibutylstannane

: 107-13-1,25014-41-9
acrylonitrile

: 157843-38-4
dibutyl(2-cyanoethyl)phenylstannane

Guidance literature:: In neat (no solvent); Sn-compd. and acrylonitrile are stirred under N2 at 80°C for 7.5h, cooling to 40°C, further stirring for 12 h; monitored by IR-spectroscopy, evapn. of excess amount of acrylonitrile under vac., distn. under vac., elem. anal.;
DOI:10.1039/DT9940002135

Reference yield: 99.0%

: 157843-38-4
dibutyl(2-cyanoethyl)phenylstannane

: 17846-68-3
azido tributyltin (IV)

: 157843-28-2
5-[2-(dibutylphenylstannyl)ethyl]-2-(tributylstannyl)tetrazole

Guidance literature:: In neat (no solvent); mixture of Sn-compds. is stirred at 104°C for 2 h; no purification possible, chromy. or distn. under vac. causes decompn.,elem. anal.;
DOI:10.1039/DT9940002135

Reference yield:

: 157843-38-4
dibutyl(2-cyanoethyl)phenylstannane

: 17846-68-3
azido tributyltin (IV)

: 157843-29-3
2,2-dibutyl-1,6,7,8-tetraaza-2-stannabicyclo[3.3.0]octa-5,7-diene

: 960-16-7
tributylphenylstannane

Guidance literature:: Multi-step reaction with 2 steps

1: neat (no solvent)

2: neat (no solvent)

In neat (no solvent);
DOI:10.1039/DT9940002135