2-((tert-Butoxycarbonyl)amino)propane-1,3-diyl dimethanesulfonate

Base Information

Chemical Name:2-((tert-Butoxycarbonyl)amino)propane-1,3-diyl dimethanesulfonate
CAS No.:213475-70-8
Molecular Formula:C₁₀H₂₁NO₈S₂
Molecular Weight:347.411
Hs Code.:
DSSTox Substance ID:DTXSID70447463
Nikkaji Number:J2.605.040E
Wikidata:Q82266342

Synonyms:213475-70-8;2-((tert-Butoxycarbonyl)amino)propane-1,3-diyl dimethanesulfonate;tert-butyl N-[1,3-bis(methanesulfonyloxy)propan-2-yl]carbamate;[2-[(2-methylpropan-2-yl)oxycarbonylamino]-3-methylsulfonyloxypropyl] methanesulfonate;2-(Boc-amino)propane-1,3-diyl Dimethanesulfonate;2-[(tert-Butoxycarbonyl)amino]propane-1,3-diyl dimethanesulfonate;N-boc-serinol dimesylate;SCHEMBL2013068;DTXSID70447463;OQZLCYFJSRPMBB-UHFFFAOYSA-N;2-((tert-Butoxycarbonyl)amino)propane-1,3-diyldimethanesulfonate;MFCD18325181;AKOS015950313;SY193026;CS-0217770;FT-0686003;EN300-84184;F53316;J-505270;N-(tert-butyloxycarbonyl)-2-amino-1,3-propanediol dimesylate;1-(Mesyloxymethyl)-2-(mesyloxy)ethylcarbamic acid tert-butyl ester

Suppliers and Price of 2-((tert-Butoxycarbonyl)amino)propane-1,3-diyl dimethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Synthonix
2-((tert-Butoxycarbonyl)amino)propane-1,3-diyldimethanesulfonate 95%+
5g
$ 1800.00

Synthonix
2-((tert-Butoxycarbonyl)amino)propane-1,3-diyldimethanesulfonate 95%+
1g
$ 480.00

American Custom Chemicals Corporation
2-((TERT-BUTOXYCARBONYL)AMINO)PROPANE-1,3-DIYL DIMETHANE SULFONATE 95.00%
5MG
$ 495.44

AK Scientific
2-((tert-Butoxycarbonyl)amino)propane-1,3-diyldimethanesulfonate
5g
$ 1275.00

Total 7 raw suppliers

Chemical Property of 2-((tert-Butoxycarbonyl)amino)propane-1,3-diyl dimethanesulfonate

Chemical Property:

XLogP3:-0.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:9
Exact Mass:347.07085898
Heavy Atom Count:21
Complexity:499

Purity/Quality:

98%min ^*data from raw suppliers

2-((tert-Butoxycarbonyl)amino)propane-1,3-diyldimethanesulfonate 95%+ ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NC(COS(=O)(=O)C)COS(=O)(=O)C

Technology Process of 2-((tert-Butoxycarbonyl)amino)propane-1,3-diyl dimethanesulfonate

There total 3 articles about 2-((tert-Butoxycarbonyl)amino)propane-1,3-diyl dimethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 125414-41-7
N-Boc-serinol

: 124-63-0
methanesulfonyl chloride

: 213475-70-8
methanesulfonic acid 2-tert-butoxycarbonylamino-3-methanesulfonyloxypropylester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 213475-70-8
methanesulfonic acid 2-tert-butoxycarbonylamino-3-methanesulfonyloxypropylester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / ethanol / 1 h / Ambient temperature

2: 82 percent / Et₃N / CH₂Cl₂ / 1.) 0 deg C, 1 h, 2.) r.t., 30 min

With triethylamine; In ethanol; dichloromethane;
DOI:10.1055/s-1998-2128

Reference yield:

: 2766-43-0
N-tert-butyloxycarbonyl-L-serine methyl ester

: 213475-70-8
methanesulfonic acid 2-tert-butoxycarbonylamino-3-methanesulfonyloxypropylester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 24 h / 0 - 20 °C

2: triethylamine / dichloromethane / 2 h / 0 - 20 °C

With sodium tetrahydroborate; triethylamine; In methanol; dichloromethane;
DOI:10.1039/c7nj03999a