1-(benzylidenamino)-3-(diethylamino)-2-methylindene

Base Information

Chemical Name:1-(benzylidenamino)-3-(diethylamino)-2-methylindene
CAS No.:136185-11-0
Molecular Formula:C₂₁H₂₄N₂
Molecular Weight:304.435
Hs Code.:

Synonyms:

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Chemical Property of 1-(benzylidenamino)-3-(diethylamino)-2-methylindene

Chemical Property:

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Technology Process of 1-(benzylidenamino)-3-(diethylamino)-2-methylindene

There total 4 articles about 1-(benzylidenamino)-3-(diethylamino)-2-methylindene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: W(CO)5(C(C₆H₅)NCH(C₆H₅))

: 4231-35-0
methyl(diethylamino)acetylene

: 136185-11-0
1-(benzylidenamino)-3-(diethylamino)-2-methylindene

: 136185-10-9
pentacarbonyl{3-(diethylamino)-4-methyl-2,5-diphenyl-2H-pyrrol}tungsten

: 136235-70-6
pentacarbonyl{(2E)-1-(diethylamino)-2-methyl-3,5-diphenyl-4-azapenta-2,4-dienylidene}tungsten

: 136185-07-4
pentacarbonyl{(2Z)-1-(diethylamino)-2-methyl-3,5-diphenyl-4-azapenta-2,4-dienylidene}tungsten

Guidance literature:: In tetrahydrofuran; under inert gas; to the W-complex was added the propine in petroleum ether at 20°C; stirring for h at -20°C;; decanted; washed 2 times with petroleum ether; dried (15 Torr/20°C); crystals from petroleum ether/CH2Cl2; mother liquor chromatographed; elution with petroleum ether/CH2Cl2 ; elem. anal.; ratio of products depending on reaction conditions;

Reference yield:

: 100-52-7
benzaldehyde

: 136185-11-0
1-(benzylidenamino)-3-(diethylamino)-2-methylindene

: 136185-10-9
pentacarbonyl{3-(diethylamino)-4-methyl-2,5-diphenyl-2H-pyrrol}tungsten

Guidance literature:: Multi-step reaction with 2 steps

1: TiCl₄; NEt₃ / dichloromethane

2: tetrahydrofuran

With TiCl₄; NEt₃; In tetrahydrofuran; dichloromethane;

Reference yield:

: pentacarbonyl(α-aminobenzylidene)tungsten

: 136185-11-0
1-(benzylidenamino)-3-(diethylamino)-2-methylindene

: 136185-10-9
pentacarbonyl{3-(diethylamino)-4-methyl-2,5-diphenyl-2H-pyrrol}tungsten

Guidance literature:: Multi-step reaction with 2 steps

1: TiCl₄; NEt₃ / dichloromethane

2: tetrahydrofuran

With TiCl₄; NEt₃; In tetrahydrofuran; dichloromethane;