Pd(CH₃)ClC₆H₅PC₁₆H₂₈N₂O₄

Base Information

• Chemical Name: Pd(CH₃)ClC₆H₅PC₁₆H₂₈N₂O₄
• CAS No.: 353797-48-5
• Molecular Formula: C₂₃H₃₆ClN₂O₄PPd
• Molecular Weight: 577.397
• Mol file: 353797-48-5.mol

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Chemical Property of Pd(CH₃)ClC₆H₅PC₁₆H₂₈N₂O₄

Chemical Property:

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Technology Process of Pd(CH₃)ClC₆H₅PC₁₆H₂₈N₂O₄

There total 1 articles about Pd(CH₃)ClC₆H₅PC₁₆H₂₈N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

chloromethyl(1,5-cyclooctadiene)palladium(II) + bis(4,4-dimethyl-2-(1-hydroxy-1-methylethyl)-4,5-dihydrooxazole)phenylphosphonite (286407-90-7) → Pd(CH3)ClC6H5PC16H28N2O4 (353797-48-5)

Guidance literature:

In dichloromethane; byproducts: 1,5-cyclooctadiene; (N2); stirring a soln. of palladium complex and ligand in CH2Cl2 overnight; evapn., washing with Et2O, drying in vac.; elem. anal.;

DOI:10.1021/om010165w

Reference yield:

Pd(CH3)ClC6H5PC16H28N2O4 (353797-48-5) + silver trifluoromethanesulfonate (2923-28-6) → [Pd(CH3)C6H5PC16H28N2O4](1+)*CF3SO3(1-)=[Pd(CH3)C6H5PC16H28N2O4]OSO2CF3

Guidance literature:

In dichloromethane;

DOI:10.1021/om010165w

upstream raw materials:

bis(4,4-dimethyl-2-(1-hydroxy-1-methylethyl)-4,5-dihydrooxazole)phenylphosphonite