Mo(N(2,6-diisopropylphenyl)(ethylene)(η1-2-mesitylpyrrolide)2

Base Information

Chemical Name:Mo(N(2,6-diisopropylphenyl)(ethylene)(η1-2-mesitylpyrrolide)2
CAS No.:1259547-25-5
Molecular Formula:C₄₀H₄₉MoN₃
Molecular Weight:667.789
Hs Code.:

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Chemical Property of Mo(N(2,6-diisopropylphenyl)(ethylene)(η1-2-mesitylpyrrolide)2

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Technology Process of Mo(N(2,6-diisopropylphenyl)(ethylene)(η1-2-mesitylpyrrolide)2

There total 1 articles about Mo(N(2,6-diisopropylphenyl)(ethylene)(η1-2-mesitylpyrrolide)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 74-85-1
ethene

: Mo(N(2,6-diisopropylphenyl)(CHCMe2Ph)(η1-2-mesitylpyrrolide)2

: 1259547-25-5
Mo(N(2,6-diisopropylphenyl)(ethylene)(η1-2-mesitylpyrrolide)2

Guidance literature:: In benzene; byproducts: CH2CHCMe2Ph; benzene was added to a Schlenk flask charged with Mo-contg. compd. (1.302 mmol); the soln. was degassed via 3 freeze-pump-thaw cycles and exposed to ethylene (1 atm); heating at 60°C for 4 d; the volatiles were removed under vac.; pentane and Et2O were added to the residue; the solid was collected and dried in vac. for 1 h; elem. anal.;
DOI:10.1021/om101003v

Reference yield: 41.0%

: 60-29-7,927820-24-4
diethyl ether

: 920-66-1
1,1,1,3',3',3'-hexafluoro-propanol

: 1259547-25-5
Mo(N(2,6-diisopropylphenyl)(ethylene)(η1-2-mesitylpyrrolide)2

: 1259547-15-3
Mo(N(2,6-diisopropylphenyl)(ethylene)(hexafluoroisopropanol-H)2(diethyl ether)

Guidance literature:: In diethyl ether; byproducts: 2,2,5-dimethylpyrrole; Mo-contg. compd. (0.301 mmol) in Et2O were added to a scintillation vial; (CF3)2CHOH (0.703 mmol) was added in portions; stirring for 30 min; the mixt. was filtered through glass wool; the filtrate was concd. in vac.; standing the soln. at -27°C for 1 d; elem. anal.;
DOI:10.1021/om101003v