(2-SC₆H₄NC(CF₃)CH₂C(CF₃)NC₆H₄S-2)SbPh

Base Information

Chemical Name:(2-SC₆H₄NC(CF₃)CH₂C(CF₃)NC₆H₄S-2)SbPh
CAS No.:357626-39-2
Molecular Formula:C₂₃H₁₅F₆N₂S₂Sb
Molecular Weight:619.258
Hs Code.:

(2-SC<sub>6</sub>H<sub>4</sub>NC(CF<sub>3</sub>)CH<sub>2</sub>C(CF<sub>3</sub>)NC<sub>6</sub>H<sub>4</sub>S-2)SbPh

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Chemical Property of (2-SC₆H₄NC(CF₃)CH₂C(CF₃)NC₆H₄S-2)SbPh

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Technology Process of (2-SC₆H₄NC(CF₃)CH₂C(CF₃)NC₆H₄S-2)SbPh

There total 1 articles about (2-SC₆H₄NC(CF₃)CH₂C(CF₃)NC₆H₄S-2)SbPh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 331251-64-0
2-HSC₆H₄NC(CF₃)CH₂C(CF₃)NC₆H₄SH-2

: 603-36-1
triphenylantimony

: 357626-39-2
(2-SC₆H₄NC(CF₃)CH₂C(CF₃)NC₆H₄S-2)SbPh

Guidance literature:: In benzene; byproducts: C6H6; C6H6 soln. of Ph3Sb was added to thiol in 1:2 molar ratio, soln. was refluxed for 5-6 h, with exclusion of moisture; solvent was removed in vac., residue was dissolved in C6H6, petroleum ether (40-60 °C) was added slowly till a viscous compd. began to separate, soln. was kept overnight at about -10 °C, solvent was decanted, drying in vac., elem. anal.;
DOI:10.1081/SIM-100002228