C₂₀H₃₀F₂N₂O₂

Base Information

Chemical Name:C₂₀H₃₀F₂N₂O₂
CAS No.:1292321-32-4
Molecular Formula:C₂₀H₃₀F₂N₂O₂
Molecular Weight:368.467
Hs Code.:

C<sub>20</sub>H<sub>30</sub>F<sub>2</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₂₀H₃₀F₂N₂O₂

Chemical Property:

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Technology Process of C₂₀H₃₀F₂N₂O₂

There total 27 articles about C₂₀H₃₀F₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1292321-39-1
C₁₉H₂₅F₂NO₃

: 593-51-1
methylamine hydrochloride

: 1292321-32-4
C₂₀H₃₀F₂N₂O₂

: 1292321-46-0
C₂₀H₃₀F₂N₂O₂

Guidance literature:: With sodium cyanoborohydride; acetic acid; triethylamine; In methanol; at 20 ℃; optical yield given as %de;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1292321-32-4
C₂₀H₃₀F₂N₂O₂

Guidance literature:: Multi-step reaction with 11 steps

1: sodium hydride / tetrahydrofuran / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethanol

3: water; potassium hydroxide / ethanol / 20 °C

4: triethylamine / diethyl ether / 20 °C

5: n-butyllithium / tetrahydrofuran / -78 °C

6: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C

7: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C

8: hydrogenchloride / tetrahydrofuran; water / 20 °C

9: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 110 °C

10: chloro-trimethyl-silane / dichloromethane / 20 °C

11: sodium cyanoborohydride; acetic acid; triethylamine / methanol / 20 °C

With hydrogenchloride; n-butyllithium; chloro-trimethyl-silane; diphenyl phosphoryl azide; palladium 10% on activated carbon; water; hydrogen; dihydrogen peroxide; sodium hexamethyldisilazane; sodium hydride; sodium cyanoborohydride; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; potassium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; toluene; 9: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: C₂₂H₂₃F₂NO₂

: 1292321-32-4
C₂₀H₃₀F₂N₂O₂

Guidance literature:: Multi-step reaction with 7 steps

1: chloro-trimethyl-silane / dichloromethane / 20 °C

2: 20% palladium hydroxide on carbon; hydrogen / ethyl acetate

3: 1H-imidazole; zinc azide * 2 pyridine; triphenylphosphine; diethylazodicarboxylate / dichloromethane / 20 °C

4: palladium 10% on activated carbon; hydrogen / ethyl acetate

5: sodium cyanoborohydride / methanol / 20 °C

6: sodium cyanoborohydride / methanol / 20 °C

7: palladium 10% on activated carbon; hydrogen; acetic acid / ethanol

With 1H-imidazole; chloro-trimethyl-silane; zinc azide * 2 pyridine; 20% palladium hydroxide on carbon; palladium 10% on activated carbon; hydrogen; sodium cyanoborohydride; acetic acid; triphenylphosphine; diethylazodicarboxylate; In methanol; ethanol; dichloromethane; ethyl acetate;
DOI:10.1016/j.bmcl.2010.12.060