3-(1,3-Dioxolan-2-yl)propyl 1-methyl-5((3((S)-phenyl((((R)-quinuclidin-3-yloxy)carbonyl)amino)methyl)phenoxy)methyl)-1H-pyrazole-3-carboxylate

Base Information

Chemical Name:3-(1,3-Dioxolan-2-yl)propyl 1-methyl-5((3((S)-phenyl((((R)-quinuclidin-3-yloxy)carbonyl)amino)methyl)phenoxy)methyl)-1H-pyrazole-3-carboxylate
CAS No.:1613414-69-9
Molecular Formula:C₃₃H₄₀N₄O₇
Molecular Weight:604.703
Hs Code.:

3-(1,3-Dioxolan-2-yl)propyl 1-methyl-5((3((S)-phenyl((((R)-quinuclidin-3-yloxy)carbonyl)amino)methyl)phenoxy)methyl)-1H-pyrazole-3-carboxylate

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Chemical Property of 3-(1,3-Dioxolan-2-yl)propyl 1-methyl-5((3((S)-phenyl((((R)-quinuclidin-3-yloxy)carbonyl)amino)methyl)phenoxy)methyl)-1H-pyrazole-3-carboxylate

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Technology Process of 3-(1,3-Dioxolan-2-yl)propyl 1-methyl-5((3((S)-phenyl((((R)-quinuclidin-3-yloxy)carbonyl)amino)methyl)phenoxy)methyl)-1H-pyrazole-3-carboxylate

There total 9 articles about 3-(1,3-Dioxolan-2-yl)propyl 1-methyl-5((3((S)-phenyl((((R)-quinuclidin-3-yloxy)carbonyl)amino)methyl)phenoxy)methyl)-1H-pyrazole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1613414-00-8
4-((3-((S)-phenyl(((((R)-quinuclidin-3-yl)oxy)carbonyl)amino)methyl)phenoxy)methyl)benzoic acid

: 1613414-69-9
3-(1,3-Dioxolan-2-yl)propyl 1-methyl-5((3((S)-phenyl((((R)-quinuclidin-3-yloxy)carbonyl)amino)methyl)phenoxy)methyl)-1H-pyrazole-3-carboxylate

Guidance literature:

Reference yield:

: 6136-67-0
3-methoxybenzophenone

: 1613414-69-9
3-(1,3-Dioxolan-2-yl)propyl 1-methyl-5((3((S)-phenyl((((R)-quinuclidin-3-yloxy)carbonyl)amino)methyl)phenoxy)methyl)-1H-pyrazole-3-carboxylate

Guidance literature:: Multi-step reaction with 9 steps

1: hydrogen bromide

2: water; ethanol; formamide

3: methanol

4: N-ethyl-N,N-diisopropylamine; potassium carbonate / methanol; ethyl acetate; dichloromethane; 2-Methylpentane

5: potassium carbonate / acetonitrile

6: hydrogenchloride / methanol; 1,4-dioxane

7: ethyl acetate; water; pyridine

8: hydrogenchloride; lithium hydroxide / tetrahydrofuran; ethanol

With hydrogenchloride; lithium hydroxide; hydrogen bromide; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; pyridine; methanol; ethanol; 2-Methylpentane; dichloromethane; water; formamide; ethyl acetate; acetonitrile;

Reference yield:

: 13020-57-0
3-hydroxybenzophenone

: 1613414-69-9
3-(1,3-Dioxolan-2-yl)propyl 1-methyl-5((3((S)-phenyl((((R)-quinuclidin-3-yloxy)carbonyl)amino)methyl)phenoxy)methyl)-1H-pyrazole-3-carboxylate

Guidance literature:: Multi-step reaction with 8 steps

1: water; ethanol; formamide

2: methanol

3: N-ethyl-N,N-diisopropylamine; potassium carbonate / methanol; ethyl acetate; dichloromethane; 2-Methylpentane

4: potassium carbonate / acetonitrile

5: hydrogenchloride / methanol; 1,4-dioxane

6: ethyl acetate; water; pyridine

7: hydrogenchloride; lithium hydroxide / tetrahydrofuran; ethanol

With hydrogenchloride; lithium hydroxide; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; pyridine; methanol; ethanol; 2-Methylpentane; dichloromethane; water; formamide; ethyl acetate; acetonitrile;