trans-1-hydroxymethyl-2-chlorocyclohexane

Base Information

• Chemical Name: trans-1-hydroxymethyl-2-chlorocyclohexane
• CAS No.: 7639-12-5
• Molecular Formula: C₇H₁₃ClO
• Molecular Weight: 148.633

Synonyms:

Chemical Property of trans-1-hydroxymethyl-2-chlorocyclohexane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of trans-1-hydroxymethyl-2-chlorocyclohexane

There total 3 articles about trans-1-hydroxymethyl-2-chlorocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

di(trans-2-chlorocyclohexylmethyl)formal (7639-16-9) → trans-1-hydroxymethyl-2-chlorocyclohexane (7639-12-5,18289-55-9,77369-76-7)

Guidance literature:

With methanol;

DOI:10.1007/BF00957243

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + cyclohexene (110-83-8) → trans-1-hydroxymethyl-2-chlorocyclohexane (7639-12-5,18289-55-9,77369-76-7)

Guidance literature:

Multistep reaction; (i) HCl, (ii) MeOH, aq. HCl;

DOI:10.1021/jo00834a021

Reference yield:

cyclohexene (110-83-8) → trans-1-hydroxymethyl-2-chlorocyclohexane (7639-12-5,18289-55-9,77369-76-7)

Guidance literature:

With hydrogenchloride; formaldehyd;

upstream raw materials:

cyclohexene

di(trans-2-chlorocyclohexylmethyl)formal

formaldehyd

Downstream raw materials:

3-hydroxymethylcyclohexene

2-(hydroxymethyl)cyclohexanol

cyclohexene

cyclohexylmethyl alcohol

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