C₅₄H₆₀F₃N₃O₇Si

Base Information

Chemical Name:C₅₄H₆₀F₃N₃O₇Si
CAS No.:1359024-16-0
Molecular Formula:C₅₄H₆₀F₃N₃O₇Si
Molecular Weight:948.167
Hs Code.:

C<sub>54</sub>H<sub>60</sub>F<sub>3</sub>N<sub>3</sub>O<sub>7</sub>Si

Synonyms:

Suppliers and Price of C₅₄H₆₀F₃N₃O₇Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₄H₆₀F₃N₃O₇Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₄H₆₀F₃N₃O₇Si

There total 16 articles about C₅₄H₆₀F₃N₃O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50868-73-0
2-methoxy-6-methylbenzeneamine

: 1359024-16-0
C₅₄H₆₀F₃N₃O₇Si

Guidance literature:: Multi-step reaction with 17 steps

1.1: bromine; acetic acid / methanol / 2 h / 20 °C / Cooling with ice

2.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C

2.2: 4 h / 0 - 50 °C

3.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / -78 - 20 °C

3.2: 1 h / 20 °C

4.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C

4.2: pH 1

5.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

6.1: triethylamine / dmap / 1 h / 20 °C

7.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

7.2: 0.33 h / 20 °C

8.1: potassium carbonate / acetone / 20 °C

9.1: n-butyllithium / tetrahydrofuran; hexanes / -100 - -96 °C

9.2: 1 h / -92 - -78 °C

9.3: 0 °C

10.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C

11.1: methanol; sodium tetrahydroborate / dichloromethane / 1.08 h / 0 - 20 °C

12.1: dmap / dichloromethane / 20 °C

13.1: iodine; silver trifluoroacetate / chloroform / 20 °C

14.1: copper(l) iodide / N,N-dimethyl-formamide / 72 h / 80 °C / Sealed flask

15.1: hydrogenchloride / 1,4-dioxane / 20 °C

15.2: 20 °C

16.1: potassium carbonate / acetone / 3 h / 20 - 50 °C

17.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diisopropylamine / tetrahydrofuran; hexanes / 0.67 h / -78 - -70 °C

17.2: -100 - -90 °C

With hydrogenchloride; methanol; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; copper(l) iodide; n-butyllithium; 2-methyl-but-2-ene; oxalyl dichloride; N,N,N,N,-tetramethylethylenediamine; bromine; iodine; silver trifluoroacetate; boron tribromide; diisobutylaluminium hydride; potassium carbonate; acetic acid; triethylamine; diisopropylamine; trifluoroacetic acid; sodium nitrite; dmap; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol;

Reference yield:

: 877149-05-8
4-bromo-2-methoxy-6-methyl-benzonitrile

: 1359024-16-0
C₅₄H₆₀F₃N₃O₇Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / -78 - 20 °C

1.2: 1 h / 20 °C

2.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C

2.2: pH 1

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

4.1: triethylamine / dmap / 1 h / 20 °C

5.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

5.2: 0.33 h / 20 °C

6.1: potassium carbonate / acetone / 20 °C

7.1: n-butyllithium / tetrahydrofuran; hexanes / -100 - -96 °C

7.2: 1 h / -92 - -78 °C

7.3: 0 °C

8.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C

9.1: methanol; sodium tetrahydroborate / dichloromethane / 1.08 h / 0 - 20 °C

10.1: dmap / dichloromethane / 20 °C

11.1: iodine; silver trifluoroacetate / chloroform / 20 °C

12.1: copper(l) iodide / N,N-dimethyl-formamide / 72 h / 80 °C / Sealed flask

13.1: hydrogenchloride / 1,4-dioxane / 20 °C

13.2: 20 °C

14.1: potassium carbonate / acetone / 3 h / 20 - 50 °C

15.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diisopropylamine / tetrahydrofuran; hexanes / 0.67 h / -78 - -70 °C

15.2: -100 - -90 °C

With hydrogenchloride; methanol; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; copper(l) iodide; n-butyllithium; 2-methyl-but-2-ene; oxalyl dichloride; N,N,N,N,-tetramethylethylenediamine; iodine; silver trifluoroacetate; boron tribromide; diisobutylaluminium hydride; potassium carbonate; triethylamine; diisopropylamine; trifluoroacetic acid; dmap; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; hexanes; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol;

Reference yield:

: 877149-08-1
4-bromo-2-methoxy-6-methyl-benzoic acid

: 1359024-16-0
C₅₄H₆₀F₃N₃O₇Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

2.1: triethylamine / dmap / 1 h / 20 °C

3.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

3.2: 0.33 h / 20 °C

4.1: potassium carbonate / acetone / 20 °C

5.1: n-butyllithium / tetrahydrofuran; hexanes / -100 - -96 °C

5.2: 1 h / -92 - -78 °C

5.3: 0 °C

6.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C

7.1: methanol; sodium tetrahydroborate / dichloromethane / 1.08 h / 0 - 20 °C

8.1: dmap / dichloromethane / 20 °C

9.1: iodine; silver trifluoroacetate / chloroform / 20 °C

10.1: copper(l) iodide / N,N-dimethyl-formamide / 72 h / 80 °C / Sealed flask

11.1: hydrogenchloride / 1,4-dioxane / 20 °C

11.2: 20 °C

12.1: potassium carbonate / acetone / 3 h / 20 - 50 °C

13.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diisopropylamine / tetrahydrofuran; hexanes / 0.67 h / -78 - -70 °C

13.2: -100 - -90 °C

With hydrogenchloride; methanol; sodium tetrahydroborate; copper(l) iodide; n-butyllithium; oxalyl dichloride; N,N,N,N,-tetramethylethylenediamine; iodine; silver trifluoroacetate; boron tribromide; potassium carbonate; triethylamine; diisopropylamine; trifluoroacetic acid; dmap; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; hexanes; dichloromethane; chloroform; N,N-dimethyl-formamide; acetone;