C₅₄H₅₀N₂P₂

Base Information

• Chemical Name: C₅₄H₅₀N₂P₂
• CAS No.: 1447832-53-2
• Molecular Formula: C₅₄H₅₀N₂P₂
• Molecular Weight: 788.952
• Mol file: 1447832-53-2.mol

Synonyms:

Chemical Property of C₅₄H₅₀N₂P₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₄H₅₀N₂P₂

There total 3 articles about C₅₄H₅₀N₂P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C54H46N2O2P2 (1447832-51-0) → C54H50N2P2 (1447832-53-2)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 5h; Reflux;

DOI:10.1002/cctc.201200590

Reference yield:

benzaldehyde (100-52-7) → C54H50N2P2 (1447832-53-2)

Guidance literature:

Multi-step reaction with 4 steps

1: methanol / Reflux

2: sodium tetrahydroborate / 0 °C / Reflux

3: chlorophosphoric acid diphenyl ester; triethylamine / dichloromethane / 0 - 25 °C

4: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / Reflux

With sodium tetrahydroborate; lithium aluminium tetrahydride; triethylamine; chlorophosphoric acid diphenyl ester; In tetrahydrofuran; methanol; dichloromethane;

DOI:10.1002/cctc.201200590

Reference yield:

N,N'-bis(benzyliden)ethylendiamine (104-71-2) → C54H50N2P2 (1447832-53-2)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium tetrahydroborate / 0 °C / Reflux

2: chlorophosphoric acid diphenyl ester; triethylamine / dichloromethane / 0 - 25 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / Reflux

With sodium tetrahydroborate; lithium aluminium tetrahydride; triethylamine; chlorophosphoric acid diphenyl ester; In tetrahydrofuran; dichloromethane;

DOI:10.1002/cctc.201200590

upstream raw materials:

N,N'-bis(benzyliden)ethylendiamine

C₅₄H₄₆N₂O₂P₂

benzaldehyde

Downstream raw materials:

C₅₆H₅₃ClN₃P₂Ru⁽¹⁺⁾*Cl^(1-)