trans-trans-di(Cl)bis(2-(m-tolylazo)pyridine)ruthenium(II)

Base Information

Chemical Name:trans-trans-di(Cl)bis(2-(m-tolylazo)pyridine)ruthenium(II)
CAS No.:81600-80-8
Molecular Formula:C₂₄H₂₂Cl₂N₆Ru
Molecular Weight:566.455
Hs Code.:

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Chemical Property of trans-trans-di(Cl)bis(2-(m-tolylazo)pyridine)ruthenium(II)

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Technology Process of trans-trans-di(Cl)bis(2-(m-tolylazo)pyridine)ruthenium(II)

There total 1 articles about trans-trans-di(Cl)bis(2-(m-tolylazo)pyridine)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 14898-67-0
ruthenium(III) chloride trihydrate

: 131972-14-0
{Ag(2-(m-tolylazo)pyridine)2}ClO₄

: cis-trans-cis-dichlorobis(2-(3'-methylphenylazo)pyridine)ruthenium(II)

: 105881-11-6,648928-36-3,77321-09-6,81600-80-8,84049-23-0
trans-trans-di(Cl)bis(2-(m-tolylazo)pyridine)ruthenium(II)

: cis,cis-RuCl₂(2-(m-toylazo)pyridine)2

Guidance literature:: In methanol; byproducts: silver chloride; heating (water bath, 40°C, 15 min, Ru compd. / Ag compd. 1/1); filtration, washing (MeOH), drying (vac.), extn. (CH2Cl2, removal AgCl), crystn. (hexane), filtrates and washings concd., pptn. (H2O), drying, chromy. (silica gel, CH2Cl2/CH3CN);
DOI:10.1039/DT9910003249

Reference yield: 95.0%

: 131972-14-0
{Ag(2-(m-tolylazo)pyridine)2}ClO₄

: 81600-80-8
RuCl₂(2-(m-tolylazo)pyridine)2

: sodium perchlorate

: 87014-42-4
2-(3-methylphenylazo)pyridine

: 139242-61-8
{Ru(2-(m-tolylazo)pyridine)3}(ClO₄)2*H₂O

Guidance literature:: In methanol; byproducts: AgCl; heated to reflux for 15 min; cooled, filtered, concd., addn. of an aq. soln. of NaClO4, pptn. filtered off, washed with diethyl ether, recrystn. (water or water-methanol 9:1); elem. anal.;

Reference yield: 85.0%

: 86783-78-0
{Ag(2,2'-bipyridine)2}ClO₄

: 81600-80-8
RuCl₂(2-(m-tolylazo)pyridine)2

: sodium perchlorate

: 139342-07-7
{Ru(2,2'-bipyridine)(2-(m-tolylazo)pyridine)2}(ClO₄)2*H₂O

Guidance literature:: In methanol; byproducts: AgCl; heated to reflux for 15 min; cooled, filtered, concd., addn. of an aq. soln. of NaClO4, pptn. filtered off, washed with diethyl ether, recrystn. (water or water-methanol 9:1); elem. anal.;