C₃₅H₅₂N₂O₅

Base Information Edit

Chemical Name:C₃₅H₅₂N₂O₅
CAS No.:1579830-78-6
Molecular Formula:C₃₅H₅₂N₂O₅
Molecular Weight:580.808
Hs Code.:
Mol file:1579830-78-6.mol

C<sub>35</sub>H<sub>52</sub>N<sub>2</sub>O<sub>5</sub>

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Chemical Property of C₃₅H₅₂N₂O₅ Edit

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Technology Process of C₃₅H₅₂N₂O₅

There total 9 articles about C₃₅H₅₂N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 1579830-64-0
C₂₇H₄₃ClO₂

: 69397-93-9
N-methyl-5-methoxy-2-nitroaniline

: 1579830-78-6
C₃₅H₅₂N₂O₅

Guidance literature:: With pyridine; In toluene; at 120 ℃;
DOI:10.1002/anie.201307465

Reference yield:

: 434-13-9
Lithocholic acid

: 1579830-78-6
C₃₅H₅₂N₂O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 3.42 h / 0 °C / Inert atmosphere; Reflux

2.1: Ag₂CO₃-celite / toluene / 24 h / Reflux

3.1: N-ethyl-N,N-diisopropylamine; lithium chloride / acetonitrile / 0.25 h / 20 °C

3.2: 20 °C

4.1: lithium hydroxide / methanol; tetrahydrofuran; water / 20 °C

5.1: methanol / 0.25 h / Schlenk technique; Inert atmosphere

5.2: 3.02 h / 50 °C

6.1: 2-iodoxybenzoic acid; 4-methylmorpholine N-oxide / dimethyl sulfoxide / 20 - 61 °C / Darkness

7.1: lithium; ammonia / tert-butyl alcohol; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

8.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 0.33 h / Inert atmosphere

9.1: pyridine / toluene / 120 °C

With pyridine; lithium aluminium tetrahydride; oxalyl dichloride; 2-iodoxybenzoic acid; ammonia; lithium; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; lithium chloride; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1002/anie.201307465

Reference yield:

: 20414-15-7,101046-88-2,20414-16-8
5β-cholane-3α,24-diol

: 1579830-78-6
C₃₅H₅₂N₂O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: Ag₂CO₃-celite / toluene / 24 h / Reflux

2.1: N-ethyl-N,N-diisopropylamine; lithium chloride / acetonitrile / 0.25 h / 20 °C

2.2: 20 °C

3.1: lithium hydroxide / methanol; tetrahydrofuran; water / 20 °C

4.1: methanol / 0.25 h / Schlenk technique; Inert atmosphere

4.2: 3.02 h / 50 °C

5.1: 2-iodoxybenzoic acid; 4-methylmorpholine N-oxide / dimethyl sulfoxide / 20 - 61 °C / Darkness

6.1: lithium; ammonia / tert-butyl alcohol; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

7.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 0.33 h / Inert atmosphere

8.1: pyridine / toluene / 120 °C

With pyridine; oxalyl dichloride; 2-iodoxybenzoic acid; ammonia; lithium; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; lithium chloride; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1002/anie.201307465