N--N-methyl-hydroxylamin

Base Information

• Chemical Name: N--N-methyl-hydroxylamin
• CAS No.: 30988-30-8
• Molecular Formula: C₁₁H₁₄N₂O₄
• Molecular Weight: 238.243

Synonyms:

Chemical Property of N--N-methyl-hydroxylamin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of N--N-methyl-hydroxylamin

There total 2 articles about N--N-methyl-hydroxylamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-Methylhydroxylamine (593-77-1) + N-(benzyloxycarbonyl)glycyl chloride (15050-24-5) → N--N-methyl-hydroxylamin (30988-30-8)

Guidance literature:

With pyridine; In tetrahydrofuran;

DOI:10.1002/hlca.19700530845

Reference yield:

N-Methylhydroxylamine (593-77-1) + N-(Benzyloxycarbonyl)glycine (1138-80-3) → N--N-methyl-hydroxylamin (30988-30-8)

Guidance literature:

With 4-methyl-morpholine; chloro-trimethyl-silane; isobutyl chloroformate;

DOI:10.1039/b507385p

Reference yield:

3,4-dihydro-2H-pyran (110-87-2) + N--N-methyl-hydroxylamin (30988-30-8) → {[methyl-(tetrahydro-pyran-2-yloxy)-carbamoyl]-methyl}-carbamic acid benzyl ester

Guidance literature:

With toluene-4-sulfonic acid;

DOI:10.1039/b507385p

upstream raw materials:

N-Methylhydroxylamine

N-(benzyloxycarbonyl)glycyl chloride

N-(Benzyloxycarbonyl)glycine

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