N-glycine methyl ester

Base Information

Chemical Name:N-glycine methyl ester
CAS No.:131692-91-6
Molecular Formula:C₂₀H₁₆F₅NO₄
Molecular Weight:429.343
Hs Code.:

N-<m-(pentafluorobenzyloxy)-E-3-methylcinnamyl>glycine methyl ester

Synonyms:

Suppliers and Price of N-glycine methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-glycine methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-glycine methyl ester

There total 6 articles about N-glycine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 131693-35-1
m-(pentafluorobenzyloxy)-E-3-methylcinnamoyl chloride

: 131692-91-6
N-glycine methyl ester

Guidance literature:: With 4-methyl-morpholine; In acetonitrile; for 0.25h; Ambient temperature;
DOI:10.1016/S0040-4020(01)87912-6

Reference yield:

: 121-71-1
3-Hydroxyacetophenone

: 131692-91-6
N-glycine methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / aq.NaOH, tetra-n-butylammonium sulfate / CH₂Cl₂ / 3 h / Ambient temperature; similar yield with K₂CO₃ in acetone (reflux, 2 h)

2: 27 percent / xylene / 34 h / Heating

3: hydrolysis

4: 98 percent / SOCl₂ / benzene / 20 h / 90 °C

5: 60 percent / N-methylmorpholine / acetonitrile / 0.25 h / Ambient temperature

With 4-methyl-morpholine; sodium hydroxide; thionyl chloride; tetrabutylammonium sulfate; In dichloromethane; acetonitrile; xylene; benzene;
DOI:10.1016/S0040-4020(01)87912-6

Reference yield:

: 131693-26-0
m-(pentafluorobenzyloxy)acetophenone

: 131692-91-6
N-glycine methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 27 percent / xylene / 34 h / Heating

2: hydrolysis

3: 98 percent / SOCl₂ / benzene / 20 h / 90 °C

4: 60 percent / N-methylmorpholine / acetonitrile / 0.25 h / Ambient temperature

With 4-methyl-morpholine; thionyl chloride; In acetonitrile; xylene; benzene;
DOI:10.1016/S0040-4020(01)87912-6