N-acetyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamide

Base Information

Chemical Name:N-acetyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamide
CAS No.:75509-39-6
Molecular Formula:C₆₂H₇₉N₁₅O₁₅S₄
Molecular Weight:1402.66
Hs Code.:

N-acetyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamide

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-acetyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamide

Chemical Property:

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Safty Information:

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Technology Process of N-acetyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamide

There total 11 articles about N-acetyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3401-57-8
N-benzyloxycarbonyl-S-benzyl-L-cysteine succinimido-ester

: 75509-39-6
N-acetyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamide

Guidance literature:: Multi-step reaction with 9 steps

1: 85 percent / dioxane / 24 h / Ambient temperature

2: 91 percent / 45percent HBr / acetic acid / 0.83 h / 20 °C

3: 70 percent / dioxane / 24 h / Ambient temperature

4: 85 percent / 45percent HBr / acetic acid / 0.83 h / 20 °C

5: 87 percent / acetic acid; dimethylformamide / Ambient temperature

6: 45percent HBr / acetic acid / 0.83 h / 20 °C

7: 87 percent / triethylamine / dimethylformamide; acetic acid / Ambient temperature

8: 45percent HBr / acetic acid / 0.83 h / 20 °C

9: dimethylformamide / Ambient temperature

With hydrogen bromide; triethylamine; In 1,4-dioxane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/DT9800001228

Reference yield:

: 75509-30-7
N-benzyloxycarbonyl-S-benzyl-L-cysteinylglycylglycine

: 75509-39-6
N-acetyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamide

Guidance literature:: Multi-step reaction with 6 steps

1: 80 percent / N,N'-dicyclohexylcarbodi-imide / dimethylformamide / 24 h / 0 - 25 °C

2: 87 percent / acetic acid; dimethylformamide / Ambient temperature

3: 45percent HBr / acetic acid / 0.83 h / 20 °C

4: 87 percent / triethylamine / dimethylformamide; acetic acid / Ambient temperature

5: 45percent HBr / acetic acid / 0.83 h / 20 °C

6: dimethylformamide / Ambient temperature

With hydrogen bromide; triethylamine; dicyclohexyl-carbodiimide; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/DT9800001228

Reference yield:

: 75509-29-4
N-benzyloxycarbonyl-S-benzyl-L-cysteinylglycylglycine succinimido-ester

: 75509-39-6
N-acetyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamide

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / acetic acid; dimethylformamide / Ambient temperature

2: 45percent HBr / acetic acid / 0.83 h / 20 °C

3: 87 percent / triethylamine / dimethylformamide; acetic acid / Ambient temperature

4: 45percent HBr / acetic acid / 0.83 h / 20 °C

5: dimethylformamide / Ambient temperature

With hydrogen bromide; triethylamine; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/DT9800001228