C₅₅H₆₈O₇Si₂

Base Information

Chemical Name:C₅₅H₆₈O₇Si₂
CAS No.:471270-18-5
Molecular Formula:C₅₅H₆₈O₇Si₂
Molecular Weight:897.312
Hs Code.:

C<sub>55</sub>H<sub>68</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:

Suppliers and Price of C₅₅H₆₈O₇Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₅H₆₈O₇Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₅H₆₈O₇Si₂

There total 25 articles about C₅₅H₆₈O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5597-54-6
4-(3-hydroxypropyl)cyclohexanone

: 471270-18-5
C₅₅H₆₈O₇Si₂

Guidance literature:: Multi-step reaction with 15 steps

1.1: 91 percent / imidazole / dimethylformamide / 16 h / 20 °C

2.1: LDA / tetrahydrofuran / 1 h / -78 - 0 °C

2.2: 9.2 g / HMPA / tetrahydrofuran / 0.17 h / -78 °C

3.1: NaH / tetrahydrofuran / 0.5 h / 0 °C

3.2: 5.5 g / tetrahydrofuran / 1.5 h / 0 - 20 °C

4.1: 62 percent / CrCl₂ / NiCl₂ / dimethylformamide / 18 h / 50 °C

5.1: LiAlH₄ / diethyl ether / 0.5 h / 20 °C

6.1: imidazole / dimethylformamide

7.1: 83 percent / pyridine / CH₂Cl₂

8.1: 71 percent / CSA / methanol / 0 °C

9.1: 98 percent / NMO / TPAP / acetone

10.1: tetrahydrofuran / 0 °C

11.1: 87 percent / Cy₃P-RuCl₂(=CHPh)-((Ms)N-CH₂-CH₂-N(MS)) / toluene / 16 h / 70 °C

12.1: 66 percent / aq. OsO₄; DMAP / 2-methyl-propan-2-ol / 0.5 h / 20 °C

13.1: 62 percent / Dess-Martin reagent / CH₂Cl₂ / -20 - 20 °C

14.1: Cu(OAc)2 / methanol

15.1: Ag₂O / dimethylformamide

With pyridine; 1H-imidazole; chromium dichloride; dmap; osmium(VIII) oxide; lithium aluminium tetrahydride; N-methyl-2-indolinone; copper diacetate; camphor-10-sulfonic acid; sodium hydride; Dess-Martin periodane; silver(l) oxide; lithium diisopropyl amide; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tetrapropylammonium perruthennate; nickel dichloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol; 10.1: Wittig olefination;
DOI:10.1039/b202020n

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 471270-18-5
C₅₅H₆₈O₇Si₂

Guidance literature:: Multi-step reaction with 15 steps

1.1: 91 percent / imidazole / dimethylformamide / 16 h / 20 °C

2.1: LDA / tetrahydrofuran / 1 h / -78 - 0 °C

2.2: 9.2 g / HMPA / tetrahydrofuran / 0.17 h / -78 °C

3.1: NaH / tetrahydrofuran / 0.5 h / 0 °C

3.2: 5.5 g / tetrahydrofuran / 1.5 h / 0 - 20 °C

4.1: 62 percent / CrCl₂ / NiCl₂ / dimethylformamide / 18 h / 50 °C

5.1: LiAlH₄ / diethyl ether / 0.5 h / 20 °C

6.1: imidazole / dimethylformamide

7.1: 83 percent / pyridine / CH₂Cl₂

8.1: 71 percent / CSA / methanol / 0 °C

9.1: 98 percent / NMO / TPAP / acetone

10.1: tetrahydrofuran / 0 °C

11.1: 87 percent / Cy₃P-RuCl₂(=CHPh)-((Ms)N-CH₂-CH₂-N(MS)) / toluene / 16 h / 70 °C

12.1: 66 percent / aq. OsO₄; DMAP / 2-methyl-propan-2-ol / 0.5 h / 20 °C

13.1: 62 percent / Dess-Martin reagent / CH₂Cl₂ / -20 - 20 °C

14.1: Cu(OAc)2 / methanol

15.1: Ag₂O / dimethylformamide

With pyridine; 1H-imidazole; chromium dichloride; dmap; osmium(VIII) oxide; lithium aluminium tetrahydride; N-methyl-2-indolinone; copper diacetate; camphor-10-sulfonic acid; sodium hydride; Dess-Martin periodane; silver(l) oxide; lithium diisopropyl amide; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tetrapropylammonium perruthennate; nickel dichloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol; 10.1: Wittig olefination;
DOI:10.1039/b202020n

Reference yield:

: 470690-19-8
(1R,2S,4S)-1-hydroxymethyl-3,3-dimethyl-7-oxabicyclo[2.2.1]hept-5-ene-2-carboxylic acid ethyl ester

: 471270-18-5
C₅₅H₆₈O₇Si₂

Guidance literature:: Multi-step reaction with 20 steps

1.1: 91 percent / p-TsOH*H₂O / 16 h / 20 °C

2.1: disiamylborane / tetrahydrofuran / 16 h / -20 °C

2.2: 76 percent / aq. NaOH; H₂O₂ / tetrahydrofuran / 3 h

3.1: 89 percent / imidazole / CH₂Cl₂ / 16 h / 20 °C

4.1: 95 percent / LiAlH₄ / diethyl ether / 0.25 h / 20 °C

5.1: 88 percent / NMO / TPAP / acetone / 2 h

6.1: n-BuLi / tetrahydrofuran; hexane / 1 h / 0 °C

6.2: 89 percent / tetrahydrofuran / 2 h / 20 °C

7.1: 96 percent / aq. HOAc / tetrahydrofuran / 16 h / 60 °C

8.1: 83 percent / SO₃*pyridine; DMSO / CH₂Cl₂ / 3 h / 20 °C

9.1: 62 percent / CrCl₂ / NiCl₂ / dimethylformamide / 18 h / 50 °C

10.1: LiAlH₄ / diethyl ether / 0.5 h / 20 °C

11.1: imidazole / dimethylformamide

12.1: 83 percent / pyridine / CH₂Cl₂

13.1: 71 percent / CSA / methanol / 0 °C

14.1: 98 percent / NMO / TPAP / acetone

15.1: tetrahydrofuran / 0 °C

16.1: 87 percent / Cy₃P-RuCl₂(=CHPh)-((Ms)N-CH₂-CH₂-N(MS)) / toluene / 16 h / 70 °C

17.1: 66 percent / aq. OsO₄; DMAP / 2-methyl-propan-2-ol / 0.5 h / 20 °C

18.1: 62 percent / Dess-Martin reagent / CH₂Cl₂ / -20 - 20 °C

19.1: Cu(OAc)2 / methanol

20.1: Ag₂O / dimethylformamide

With pyridine; 1H-imidazole; chromium dichloride; dmap; osmium(VIII) oxide; lithium aluminium tetrahydride; n-butyllithium; N-methyl-2-indolinone; copper diacetate; pyridine-SO₃ complex; camphor-10-sulfonic acid; bis-(1,2-dimethylpropyl)borane; Dess-Martin periodane; toluene-4-sulfonic acid; acetic acid; dimethyl sulfoxide; silver(l) oxide; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tetrapropylammonium perruthennate; nickel dichloride; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol; 6.2: Wittig olefination / 15.1: Wittig olefination;
DOI:10.1039/b202020n