α,α-Divinylphenylessigsaeure

Base Information

• Chemical Name: α,α-Divinylphenylessigsaeure
• CAS No.: 70179-00-9
• Molecular Formula: C₁₂H₁₂O₂
• Molecular Weight: 188.226
• Mol file: 70179-00-9.mol

Synonyms:

Chemical Property of α,α-Divinylphenylessigsaeure

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α,α-Divinylphenylessigsaeure

There total 6 articles about α,α-Divinylphenylessigsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

α,α-Divinylphenylacetamid (70179-01-0) → α,α-Divinylphenylessigsaeure (70179-00-9)

Guidance literature:

With hydrogenchloride; isopentyl nitrite; In 1,4-dioxane;

DOI:10.1021/jo01328a044

Reference yield:

α,α-Divinylphenylacetonitril (70179-03-2) → α,α-Divinylphenylessigsaeure (70179-00-9)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂SO₄ / acetic acid

2: BF₃-Et₂O / tetrachloroethene

3: HCl, isoamylnitrite / dioxane

With hydrogenchloride; sulfuric acid; boron trifluoride diethyl etherate; isopentyl nitrite; In 1,4-dioxane; 1,1,2,2-tetrachloroethylene; acetic acid;

DOI:10.1021/jo01328a044

Reference yield:

N-tert-Butyl-α,α-divinylphenylacetamid (70179-02-1) → α,α-Divinylphenylessigsaeure (70179-00-9)

Guidance literature:

Multi-step reaction with 2 steps

1: BF₃-Et₂O / tetrachloroethene

2: HCl, isoamylnitrite / dioxane

With hydrogenchloride; boron trifluoride diethyl etherate; isopentyl nitrite; In 1,4-dioxane; 1,1,2,2-tetrachloroethylene;

DOI:10.1021/jo01328a044

upstream raw materials:

α,α-Divinylphenylacetamid

α,α-Divinylphenylacetonitril

N-tert-Butyl-α,α-divinylphenylacetamid

α,α-bis(2-hydroxyethyl)phenylacetonitrile

Downstream raw materials:

β,β-Divinyl-β-phenylethanol