α,α-Divinylphenylacetamid

Base Information

• Chemical Name: α,α-Divinylphenylacetamid
• CAS No.: 70179-01-0
• Molecular Formula: C₁₂H₁₃NO
• Molecular Weight: 187.241
• Mol file: 70179-01-0.mol

Synonyms:

Chemical Property of α,α-Divinylphenylacetamid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α,α-Divinylphenylacetamid

There total 5 articles about α,α-Divinylphenylacetamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-tert-Butyl-α,α-divinylphenylacetamid (70179-02-1) → α,α-Divinylphenylacetamid (70179-01-0)

Guidance literature:

With boron trifluoride diethyl etherate; In 1,1,2,2-tetrachloroethylene;

DOI:10.1021/jo01328a044

Reference yield:

α,α-Divinylphenylacetonitril (70179-03-2) → α,α-Divinylphenylacetamid (70179-01-0)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂SO₄ / acetic acid

2: BF₃-Et₂O / tetrachloroethene

With sulfuric acid; boron trifluoride diethyl etherate; In 1,1,2,2-tetrachloroethylene; acetic acid;

DOI:10.1021/jo01328a044

Reference yield:

α,α-bis(2-hydroxyethyl)phenylacetonitrile (10469-27-9) → α,α-Divinylphenylacetamid (70179-01-0)

Guidance literature:

Multi-step reaction with 4 steps

1: Py

2: KOtBu / dimethylsulfoxide

3: H₂SO₄ / acetic acid

4: BF₃-Et₂O / tetrachloroethene

With pyridine; sulfuric acid; boron trifluoride diethyl etherate; potassium tert-butylate; In 1,1,2,2-tetrachloroethylene; acetic acid; dimethyl sulfoxide;

DOI:10.1021/jo01328a044

upstream raw materials:

N-tert-Butyl-α,α-divinylphenylacetamid

α,α-Divinylphenylacetonitril

α,α-bis(2-hydroxyethyl)phenylacetonitrile

2-phenyl-4-vinyloxy-2-(2-vinyloxy-ethyl)-butyronitrile

Downstream raw materials:

β,β-Divinyl-β-phenylethanol

α,α-Divinylphenylessigsaeure