N-{3-[(2R,3R,4R,5S,6R)-3-Acetylamino-6-benzyloxymethyl-5-((3aS,4R,6S,7R,7aR)-4-benzyloxymethyl-7-hydroxy-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy)-4-hydroxy-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide

Base Information

Chemical Name:N-{3-[(2R,3R,4R,5S,6R)-3-Acetylamino-6-benzyloxymethyl-5-((3aS,4R,6S,7R,7aR)-4-benzyloxymethyl-7-hydroxy-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy)-4-hydroxy-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide
CAS No.:497173-07-6
Molecular Formula:C₃₆H₄₇F₃N₂O₁₂
Molecular Weight:756.771
Hs Code.:

N-{3-[(2R,3R,4R,5S,6R)-3-Acetylamino-6-benzyloxymethyl-5-((3aS,4R,6S,7R,7aR)-4-benzyloxymethyl-7-hydroxy-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy)-4-hydroxy-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide

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Suppliers and Price of N-{3-[(2R,3R,4R,5S,6R)-3-Acetylamino-6-benzyloxymethyl-5-((3aS,4R,6S,7R,7aR)-4-benzyloxymethyl-7-hydroxy-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy)-4-hydroxy-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide

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Chemical Property of N-{3-[(2R,3R,4R,5S,6R)-3-Acetylamino-6-benzyloxymethyl-5-((3aS,4R,6S,7R,7aR)-4-benzyloxymethyl-7-hydroxy-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy)-4-hydroxy-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide

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Technology Process of N-{3-[(2R,3R,4R,5S,6R)-3-Acetylamino-6-benzyloxymethyl-5-((3aS,4R,6S,7R,7aR)-4-benzyloxymethyl-7-hydroxy-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy)-4-hydroxy-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide

There total 3 articles about N-{3-[(2R,3R,4R,5S,6R)-3-Acetylamino-6-benzyloxymethyl-5-((3aS,4R,6S,7R,7aR)-4-benzyloxymethyl-7-hydroxy-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy)-4-hydroxy-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121042-74-8
3-(trifluoroacetamido)propyl 2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

: 497173-07-6
N-{3-[(2R,3R,4R,5S,6R)-3-Acetylamino-6-benzyloxymethyl-5-((3aS,4R,6S,7R,7aR)-4-benzyloxymethyl-7-hydroxy-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy)-4-hydroxy-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / AgOTf

2: MeONa / methanol

3: TsOH

With sodium methylate; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; In methanol; 2: Zemplen deacetylation;
DOI:10.1070/MC2002v012n04ABEH001591

Reference yield:

: (3-trifluoroacetamidopropyl)-2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-4-O-(2,3,4-tri-O-acetyl-6-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

: 497173-07-6
N-{3-[(2R,3R,4R,5S,6R)-3-Acetylamino-6-benzyloxymethyl-5-((3aS,4R,6S,7R,7aR)-4-benzyloxymethyl-7-hydroxy-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy)-4-hydroxy-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: MeONa / methanol

2: TsOH

With sodium methylate; toluene-4-sulfonic acid; In methanol; 1: Zemplen deacetylation;
DOI:10.1070/MC2002v012n04ABEH001591