C₃₆H₃₉NO₇

Base Information

Chemical Name:C₃₆H₃₉NO₇
CAS No.:1428770-49-3
Molecular Formula:C₃₆H₃₉NO₇
Molecular Weight:597.708
Hs Code.:

C<sub>36</sub>H<sub>39</sub>NO<sub>7</sub>

Synonyms:

Suppliers and Price of C₃₆H₃₉NO₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₆H₃₉NO₇

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₃₆H₃₉NO₇

There total 9 articles about C₃₆H₃₉NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16792-48-6
D-glucose propane-1,3-diyl dithioacetal

: 1428770-49-3
C₃₆H₃₉NO₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: dmap / pyridine / 48 h / 35 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil; N,N-dimethyl-formamide / 0.5 h / 20 °C

2.2: 20 °C

3.1: sulfuric acid; methanol / dichloromethane / 20 °C

4.1: triethylamine / dichloromethane / 0 - 20 °C

5.1: N-Bromosuccinimide / acetonitrile / 1 h / 20 °C

6.1: potassium carbonate; methanol / 3 h / 20 °C

7.1: oxalyl dichloride / dichloromethane; dimethyl sulfoxide / 0.33 h / -70 °C

7.2: 1.25 h / -70 - 20 °C

8.1: sodium hydrogencarbonate; hydroxylamine hydrochloride; methanol / 20 °C

With methanol; dmap; N-Bromosuccinimide; oxalyl dichloride; sulfuric acid; hydroxylamine hydrochloride; sodium hydride; sodium hydrogencarbonate; potassium carbonate; triethylamine; In tetrahydrofuran; pyridine; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1021/jo400130p

Reference yield:

: 2280-44-6
D-Glucose

: 1428770-49-3
C₃₆H₃₉NO₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogenchloride; water / 20 °C

2.1: dmap / pyridine / 48 h / 35 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil; N,N-dimethyl-formamide / 0.5 h / 20 °C

3.2: 20 °C

4.1: sulfuric acid; methanol / dichloromethane / 20 °C

5.1: triethylamine / dichloromethane / 0 - 20 °C

6.1: N-Bromosuccinimide / acetonitrile / 1 h / 20 °C

7.1: potassium carbonate; methanol / 3 h / 20 °C

8.1: oxalyl dichloride / dichloromethane; dimethyl sulfoxide / 0.33 h / -70 °C

8.2: 1.25 h / -70 - 20 °C

9.1: sodium hydrogencarbonate; hydroxylamine hydrochloride; methanol / 20 °C

With hydrogenchloride; methanol; dmap; N-Bromosuccinimide; oxalyl dichloride; sulfuric acid; hydroxylamine hydrochloride; water; sodium hydride; sodium hydrogencarbonate; potassium carbonate; triethylamine; In tetrahydrofuran; pyridine; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1021/jo400130p

Reference yield:

: 1427016-50-9
6-O-trityl-D-glucose propane-1,3-diyl dithioacetal

: 1428770-49-3
C₃₆H₃₉NO₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil; N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 20 °C

2.1: sulfuric acid; methanol / dichloromethane / 20 °C

3.1: triethylamine / dichloromethane / 0 - 20 °C

4.1: N-Bromosuccinimide / acetonitrile / 1 h / 20 °C

5.1: potassium carbonate; methanol / 3 h / 20 °C

6.1: oxalyl dichloride / dichloromethane; dimethyl sulfoxide / 0.33 h / -70 °C

6.2: 1.25 h / -70 - 20 °C

7.1: sodium hydrogencarbonate; hydroxylamine hydrochloride; methanol / 20 °C

With methanol; N-Bromosuccinimide; oxalyl dichloride; sulfuric acid; hydroxylamine hydrochloride; sodium hydride; sodium hydrogencarbonate; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1021/jo400130p