1,1'-Biphenyl, 3'-methoxy-2-methyl-

Base Information

Chemical Name:1,1'-Biphenyl, 3'-methoxy-2-methyl-
CAS No.:135227-03-1
Molecular Formula:C14H14O
Molecular Weight:198.265
Hs Code.:

Synonyms:.2-methyl-3'-methoxybiphenyl;3-methoxy-2'-methyl-1,1'-biphenyl;.3'-methoxy-2-methyl-biphenyl;.3'-methoxy-2-methylbiphenyl;.3-methoxy-2'-methylbiphenyl;.3-(2'-methylphenyl)anisole;

Suppliers and Price of 1,1'-Biphenyl, 3'-methoxy-2-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1,1'-Biphenyl, 3'-methoxy-2-methyl-

Chemical Property:

PSA：9.23000
LogP:3.67060

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,1'-Biphenyl, 3'-methoxy-2-methyl-

There total 1 articles about 1,1'-Biphenyl, 3'-methoxy-2-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6699-93-0
(2-methylphenyl)lithium

: 31600-88-1
m-methoxyphenyllithium

: 605-39-0
2,2'-dimethyl-1,1'-biphenyl

: 6161-50-8
3,3'-dimethoxybiphenyl

: 135227-03-1
3-methoxy-2'-methyl-1,1'-biphenyl

Guidance literature:: Yield given. Multistep reaction. Yields of byproduct given;
DOI:10.1021/ja00021a049

Reference yield: 100.0%

: 135227-03-1
3-methoxy-2'-methyl-1,1'-biphenyl

: 71965-05-4
2'-methyl-[1,1'-biphenyl]-3-ol

Guidance literature:: With boron tribromide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201103050

Reference yield:

: 135227-03-1
3-methoxy-2'-methyl-1,1'-biphenyl

: 2'-[6-(4-nitro-benzylsulfanyl)-purin-9-ylmethyl]-biphenyl-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: NBS; benzoyl peroxide / CCl₄ / 40 h / 80 °C

2.1: NaH / dimethylformamide / 0.08 h

2.2: 37 percent / dimethylformamide / 16 h / 20 °C

3.1: 22 percent / BBr₃ / CH₂Cl₂ / -78 - 20 °C

With N-Bromosuccinimide; boron tribromide; sodium hydride; dibenzoyl peroxide; In tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm049735v