diphenylacetylene(tris(dimethylphosphinomethyl)methylsilane)iron

Base Information

Chemical Name:diphenylacetylene(tris(dimethylphosphinomethyl)methylsilane)iron
CAS No.:105177-74-0
Molecular Formula:C₂₄H₃₇FeP₃Si
Molecular Weight:502.412
Hs Code.:

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Chemical Property of diphenylacetylene(tris(dimethylphosphinomethyl)methylsilane)iron

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Technology Process of diphenylacetylene(tris(dimethylphosphinomethyl)methylsilane)iron

There total 3 articles about diphenylacetylene(tris(dimethylphosphinomethyl)methylsilane)iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: {bis(tris(dimethylphosphinomethyl)methylsilane)iron}(μ-trichloro)chloride

: 501-65-5
diphenyl acetylene

: 105177-74-0
diphenylacetylene(tris(dimethylphosphinomethyl)methylsilane)iron

Guidance literature:: With sodium amalgame; In toluene; A mixt. of reagents was dissolved in toluene and added to Na/Hg; then stirred for 1 h (inert atm.);; filtered, extd. with petroleum ether, filtered, concd., cooled to -25°C; el;
DOI:10.1016/0022-328X(87)80402-3

Reference yield:

: tris(dimethylphosphinomethyl)methylsilane

: 105177-74-0
diphenylacetylene(tris(dimethylphosphinomethyl)methylsilane)iron

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane; toluene

2: sodium amalgame / toluene

With sodium amalgame; In dichloromethane; toluene;
DOI:10.1016/0022-328X(87)80402-3