Phenol, 2-(1-cyclohexen-1-yl)-

Base Information

• Chemical Name: Phenol, 2-(1-cyclohexen-1-yl)-
• CAS No.: 13524-72-6
• Molecular Formula: C12H14O
• Molecular Weight: 174.243
• DSSTox Substance ID: DTXSID90480978
• Nikkaji Number: J801.725E
• Wikidata: Q82316152
• Mol file: 13524-72-6.mol

Synonyms:13524-72-6;Phenol, 2-(1-cyclohexen-1-yl)-;cyclohexenylphenol;SCHEMBL188942;DTXSID90480978

Chemical Property of Phenol, 2-(1-cyclohexen-1-yl)-

Chemical Property:

• XLogP3: 3.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 174.104465066
• Heavy Atom Count: 13
• Complexity: 195

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(=CC1)C2=CC=CC=C2O

Technology Process of Phenol, 2-(1-cyclohexen-1-yl)-

There total 21 articles about Phenol, 2-(1-cyclohexen-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.1%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + phenol (108-95-2,27073-41-2) → 2-(1-cyclohexenyl)cyclohexanone (1502-22-3) + 1-(2-hydroxyphenyl)cyclohexene (13524-72-6) + 1,2,3,4,5,6,7,8,9,10,11,12-dodecahydrotriphenylene (1610-39-5) + 1-(2-hydroxyphenyl)-1-(4-hydroxyphenyl)cyclohexane (71401-15-5) + 3,4-butano-2H-chromene-2-spirocyclohexane (95449-01-7)

Guidance literature:

With aluminium(III) phenoxide; at 155 ℃; for 10h; Product distribution; in cumene; other solvents; other temperature;

Reference yield: 19.1%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + phenol (108-95-2,27073-41-2) → 2-(1-cyclohexenyl)cyclohexanone (1502-22-3) + 1-(4-hydroxyphenyl)-1-cyclohexene (709-08-0) + 1-(2-hydroxyphenyl)cyclohexene (13524-72-6) + 1,2,3,4,5,6,7,8,9,10,11,12-dodecahydrotriphenylene (1610-39-5) + 3,4-butano-2H-chromene-2-spirocyclohexane (95449-01-7) + 1,2,3,4,4a,9b-hexahydrodibenzo[b,d]furan (13524-79-3,151123-20-5)

Guidance literature:

With aluminium(III) phenoxide; at 180 ℃; for 10h; Product distribution; other temperature;

Reference yield: 1.9%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + phenol (108-95-2,27073-41-2) → 2-(1-cyclohexenyl)cyclohexanone (1502-22-3) + 1-(2-hydroxyphenyl)cyclohexene (13524-72-6) + 1,2,3,4,5,6,7,8,9,10,11,12-dodecahydrotriphenylene (1610-39-5) + 1-(2-hydroxyphenyl)-1-(4-hydroxyphenyl)cyclohexane (71401-15-5)

Guidance literature:

With aluminium(III) phenoxide; In various solvent(s); at 150 ℃; Further byproducts given;

upstream raw materials:

3-phenoxycyclohexene

2-(1-Hydroxy-cyclohexyl)-phenol

cyclohexanone

phenol

Downstream raw materials:

1-cyclohexenyl-2-(2-propynyloxy)benzene