Cyclohexanone, 2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-

Base Information

Chemical Name:Cyclohexanone, 2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-
CAS No.:135297-11-9
Molecular Formula:C₁₃H₂₆O₂Si
Molecular Weight:242.434
Hs Code.:
Mol file:135297-11-9.mol

Synonyms:

Suppliers and Price of Cyclohexanone, 2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Cyclohexanone, 2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Cyclohexanone, 2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-

There total 3 articles about Cyclohexanone, 2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 832131-69-8
(+/-)-cis/trans-2-{[(tert-butyl)(dimethyl)silyloxy]methyl}cyclohexanol

: 135297-11-9
C₁₃H₂₆O₂Si

Guidance literature:: With silica gel; pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 14h; Inert atmosphere;
DOI:10.1002/anie.201007135

Reference yield:

: 930-68-7
cyclohexenone

: 135297-11-9
C₁₃H₂₆O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine; magnesium / tetrahydrofuran / 14 h / 66 °C / Inert atmosphere

1.2: 6 h / 20 °C / Inert atmosphere

2.1: silica gel; pyridinium chlorochromate / dichloromethane / 14 h / 20 °C / Inert atmosphere

With iodine; silica gel; magnesium; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201007135

Reference yield:

: 140139-05-5
bromomethoxy(t-butyl)dimethylsilane

: 135297-11-9
C₁₃H₂₆O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine; magnesium / tetrahydrofuran / 14 h / 66 °C / Inert atmosphere

1.2: 6 h / 20 °C / Inert atmosphere

2.1: silica gel; pyridinium chlorochromate / dichloromethane / 14 h / 20 °C / Inert atmosphere

With iodine; silica gel; magnesium; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201007135