Technology Process of C50H71N4O10PSi
There total 4 articles about C50H71N4O10PSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 1h;
DOI:10.1021/ja300044e
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / 16 h / 0 - 20 °C
2: pyridine; silver nitrate / tetrahydrofuran / 8 h / Sonication
3: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h
With
pyridine; silver nitrate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja300044e
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
1.2: 0.5 h
2.1: trifluoroacetic acid / water / 4 h
3.1: pyridine / 16 h / 0 - 20 °C
4.1: pyridine; silver nitrate / tetrahydrofuran / 8 h / Sonication
5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h
With
pyridine; silver nitrate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja300044e