trans-(PPh₃)2(diphenylglyoxime) picolinate ruthenium(II) perchlorate

Base Information

Chemical Name:trans-(PPh₃)2(diphenylglyoxime) picolinate ruthenium(II) perchlorate
CAS No.:339149-63-2
Molecular Formula:C₅₆H₄₆N₃O₄P₂Ru*ClO₄
Molecular Weight:1087.47
Hs Code.:

trans-(PPh<sub>3</sub>)2(diphenylglyoxime) picolinate ruthenium(II) perchlorate

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Chemical Property of trans-(PPh₃)2(diphenylglyoxime) picolinate ruthenium(II) perchlorate

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Technology Process of trans-(PPh₃)2(diphenylglyoxime) picolinate ruthenium(II) perchlorate

There total 1 articles about trans-(PPh₃)2(diphenylglyoxime) picolinate ruthenium(II) perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 98-98-6
2-Picolinic acid

: 73411-48-0
(benzil-α-dioxime)dichlorobis(triphenylphosphine)ruthenium(II)

: sodium perchlorate

: 339149-63-2
trans-(PPh₃)2(diphenylglyoxime) picolinate ruthenium(II) perchlorate

Guidance literature:: With triethylamine; In ethanol; dichloromethane; water; ethanolic soln. of picolinic acid added to CH2Cl2 soln. of Ru(PPh3)2(diphenylglyoxime)Cl2; triethylamine added; heated gently to expel CH2Cl2; refluxed for 6 h; cooled to room temp.; satd. aq. soln. of NaClO4 added; solvent evapd.; solid washed thoroughly with cold water; dried in vac. over P4O10; recrystd. from dichloromethane/hexane soln.; elem. anal.;
DOI:10.1016/S0277-5387(00)00613-6