ethyl levulinate, (O-benzyloxime)

Base Information

Chemical Name:ethyl levulinate, (O-benzyloxime)
CAS No.:82578-73-2
Molecular Formula:C₁₄H₁₉NO₃
Molecular Weight:249.31
Hs Code.:

Synonyms:

Suppliers and Price of ethyl levulinate, (O-benzyloxime)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl levulinate, (O-benzyloxime)

Chemical Property:

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Technology Process of ethyl levulinate, (O-benzyloxime)

There total 3 articles about ethyl levulinate, (O-benzyloxime) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 539-88-8
4-oxopentanoic acid ethyl ester

: 82578-72-1,82578-73-2
ethyl levulinate, (O-benzyloxime)

Guidance literature:: In pyridine; ethanol; at 55 ℃; for 24h;
DOI:10.1021/ja010066+

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 82578-72-1,82578-73-2
ethyl levulinate, (O-benzyloxime)

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / 1.) aq. NaOH / methanol / 2.) room temp., 5 h

2: 1.) lithium-diisopropylamid / 1.) THF, -50 deg C to -30 deg C, 45 min; 2.) reflux, 30 min

With sodium hydroxide; lithium diisopropyl amide; In methanol;
DOI:10.1055/s-1982-29790

Reference yield:

: 101542-13-6
iodoacetone O-benzyl oxime

: 141-78-6
ethyl acetate

: 82578-72-1,82578-73-2
ethyl levulinate, (O-benzyloxime)

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -50 deg C to -30 deg C, 45 min; 2.) reflux, 30 min;
DOI:10.1055/s-1982-29790