Ni[O,O'-di-m-tolyl dithiophosphate]2

Base Information

Chemical Name:Ni[O,O'-di-m-tolyl dithiophosphate]2
CAS No.:97138-63-1
Molecular Formula:C₂₈H₂₈NiO₄P₂S₄
Molecular Weight:677.429
Hs Code.:

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Chemical Property of Ni[O,O'-di-m-tolyl dithiophosphate]2

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Technology Process of Ni[O,O'-di-m-tolyl dithiophosphate]2

There total 1 articles about Ni[O,O'-di-m-tolyl dithiophosphate]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: nickel(II) chloride hexahydrate

: 40783-16-2
O,O-di(m-tolyl)dithiophosphoric acid ammonium salt

: 97138-63-1
Ni[O,O'-di-m-tolyl dithiophosphate]2

Guidance literature:: In water; byproducts: NH4Cl; aq. suspn. of ligand added to aq. suspn. of Ni salt in 1:2 molar ratio with stirring, stirred for 3 h; filtered, washed with dried benzene; elem. anal.;
DOI:10.1016/j.poly.2005.10.022

Reference yield: 74.0%

: 366-18-7
[2,2]bipyridinyl

: 97138-63-1
bis(O,O'-di(m-tolyl)dithiophosphato)nickel(II)

: 948025-53-4
(2,2'-bipyridine)bis(O,O'-di(m-tolyl)dithiophosphato)nickel(II)

Guidance literature:: In benzene; under anhyd. conditions, N-base was added to benzene soln. of Ni-compd.; soln. was concd. in vac., Et2O was added, recrystn. from CH2Cl2/ether (1:2, v/v), elem. anal.;
DOI:10.1016/j.poly.2007.01.003

Reference yield: 73.0%

: 110-86-1
pyridine

: 97138-63-1
bis(O,O'-di(m-tolyl)dithiophosphato)nickel(II)

: 948025-50-1
bis(O,O'-di(m-tolyl)dithiophosphato)bis(pyridine)nickel(II)

Guidance literature:: In benzene; under anhyd. conditions, N-base was added to benzene soln. of Ni-compd.; soln. was concd. in vac., Et2O was added, recrystn. from CH2Cl2/ether (1:2, v/v), elem. anal.;
DOI:10.1016/j.poly.2007.01.003