acetyl protected ferrocene-substituted biphenyl ethynyl thiol

Base Information

Chemical Name:acetyl protected ferrocene-substituted biphenyl ethynyl thiol
CAS No.:918403-40-4
Molecular Formula:C₂₆H₂₀FeOS
Molecular Weight:436.357
Hs Code.:

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Chemical Property of acetyl protected ferrocene-substituted biphenyl ethynyl thiol

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Technology Process of acetyl protected ferrocene-substituted biphenyl ethynyl thiol

There total 1 articles about acetyl protected ferrocene-substituted biphenyl ethynyl thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 933779-24-9
4-iodo-4'-thioacetylbiphenyl

: 1271-47-2
ferroceneacetylene

: 918403-40-4
acetyl protected ferrocene-substituted biphenyl ethynyl thiol

Guidance literature:: With (Ph₃P)2PdCl₂; CuI; In triethylamine; (N2); std. Schlenk technique; catalytic amt. of Pd complex/CuI was addedto Fe complex and I(C6H4)2SC(O)Me in Et3N at 25°C; stirred at 50 °C for 24 h; volatiles removed (vac.); chromd. (silica gel, hexane/CH2Cl2, 3/2); evapd. (vac.); elem. anal.;
DOI:10.1016/j.jorganchem.2006.12.002