2,3,2',3'-tetra-O-benzyl-6-O-stearoyl-α,α-trehalose

Base Information

Chemical Name:2,3,2',3'-tetra-O-benzyl-6-O-stearoyl-α,α-trehalose
CAS No.:82305-39-3
Molecular Formula:C₅₈H₈₀O₁₂
Molecular Weight:969.266
Hs Code.:

Synonyms:

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Chemical Property of 2,3,2',3'-tetra-O-benzyl-6-O-stearoyl-α,α-trehalose

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Technology Process of 2,3,2',3'-tetra-O-benzyl-6-O-stearoyl-α,α-trehalose

There total 4 articles about 2,3,2',3'-tetra-O-benzyl-6-O-stearoyl-α,α-trehalose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-20-7
TREHALOSE

: 82305-39-3
2,3,2',3'-tetra-O-benzyl-6-O-stearoyl-α,α-trehalose

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / p-toluenesulfonic acid monohydrate / dimethylformamide / 2 h / 65 °C / 40 Torr / reflux

2: 1.) 50percent NaH / 1.) DMSO, 1 h, r.t.; 2.) DMSO, 2 h

3: 92 percent / 80percent aq. AcOH / 0.5 h / Heating

4: CH₂Cl₂; pyridine / Ambient temperature

With sodium hydride; toluene-4-sulfonic acid; acetic acid; In pyridine; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 18929-82-3
4,6-O-benzylidene-α-D-glucopyranosyl-(1→1)-4',6'-O-benzylidene-α-D-glucopyranoside

: 82305-39-3
2,3,2',3'-tetra-O-benzyl-6-O-stearoyl-α,α-trehalose

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 50percent NaH / 1.) DMSO, 1 h, r.t.; 2.) DMSO, 2 h

2: 92 percent / 80percent aq. AcOH / 0.5 h / Heating

3: CH₂Cl₂; pyridine / Ambient temperature

With sodium hydride; acetic acid; In pyridine; dichloromethane;

Reference yield:

: 82305-37-1
2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside

: 82305-39-3
2,3,2',3'-tetra-O-benzyl-6-O-stearoyl-α,α-trehalose

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 80percent aq. AcOH / 0.5 h / Heating

2: CH₂Cl₂; pyridine / Ambient temperature

With acetic acid; In pyridine; dichloromethane;