bis(1-phenylborinato)vanadium

Base Information

Chemical Name:bis(1-phenylborinato)vanadium
CAS No.:90857-16-2
Molecular Formula:C₂₂H₂₀B₂V
Molecular Weight:356.964
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(1-phenylborinato)vanadium

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Technology Process of bis(1-phenylborinato)vanadium

There total 1 articles about bis(1-phenylborinato)vanadium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 36534-31-3
{(C₅H₅B)C₆H₅}2Co

: 7718-98-1
vanadium(III) chloride

: 90857-16-2
bis(1-phenylborinato)vanadium

Guidance literature:: With cyanide; In acetonitrile; under N2, Co complex in MeCN subjected to decompn. with cyanide and filtered to VCl3, stirred for 24 h at room temp.; evapd. in vac., taken up in ether, filtered through Al2O3 (4% H2O), concd. in vac., layered with pentane, crystd. at -78°C, sublimed (1E-6 bar, 100°C); elem. anal.;
DOI:10.1016/0022-328X(84)80085-6