2'-Benzoyl-4'-chloro-N-sarcosinanilide

Base Information

Chemical Name:2'-Benzoyl-4'-chloro-N-sarcosinanilide
CAS No.:78823-08-2
Molecular Formula:C₂₆H₂₄ClN₃O₅
Molecular Weight:493.947
Hs Code.:

2'-Benzoyl-4'-chloro-N-<N-(benzyloxycarbonyl)glycyl>sarcosinanilide

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-Benzoyl-4'-chloro-N-sarcosinanilide

Chemical Property:

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Technology Process of 2'-Benzoyl-4'-chloro-N-sarcosinanilide

There total 1 articles about 2'-Benzoyl-4'-chloro-N-sarcosinanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57180-64-0
2-(methylamino-acetamido)-5-chloro-benzophenone

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 78823-08-2
2'-Benzoyl-4'-chloro-N-sarcosinanilide

Guidance literature:: With thionyl chloride; Yield given. Multistep reaction; 1) HMPA, -8 to -5 deg C, 15 min, 2) ethyl acetate, -5 deg C - RT, 5 h;
DOI:10.1021/jo00335a034

Reference yield:

: 78823-08-2
2'-Benzoyl-4'-chloro-N-sarcosinanilide

: 78823-16-2
6-Chloro-1-methyl-3-(methylglycylamino)-4-phenyl-2(1H)-quinolone

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH / 1) THF, -5 to 0 deg C, 15 min, 2) 0 deg C - RT, then 1 h

2: 86 percent / HBr / acetic acid / 0.25 h / Ambient temperature

With hydrogen bromide; sodium hydride; In acetic acid;
DOI:10.1021/jo00335a034

Reference yield:

: 78823-08-2
2'-Benzoyl-4'-chloro-N-sarcosinanilide

: 74-88-4
methyl iodide

: 78823-13-9
6-Chloro-1-methyl-3-amino>-4-phenyl-2(1H)-quinolone

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1) THF, -5 to 0 deg C, 15 min, 2) 0 deg C - RT, then 1 h;
DOI:10.1021/jo00335a034