8-azido-3,6-dioxaoctyl 3-O-benzyl-2-deoxy-6-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-gglucopyranosyl>-β-D-glucopyrnoside

Base Information

Chemical Name:8-azido-3,6-dioxaoctyl 3-O-benzyl-2-deoxy-6-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-gglucopyranosyl>-β-D-glucopyrnoside
CAS No.:106256-83-1
Molecular Formula:C₄₇H₆₆N₄O₂₅
Molecular Weight:1087.05
Hs Code.:

8-azido-3,6-dioxaoctyl 3-O-benzyl-2-deoxy-6-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-gglucopyranosyl>-β-D-glucopyrnoside

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Chemical Property of 8-azido-3,6-dioxaoctyl 3-O-benzyl-2-deoxy-6-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-gglucopyranosyl>-β-D-glucopyrnoside

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Technology Process of 8-azido-3,6-dioxaoctyl 3-O-benzyl-2-deoxy-6-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-gglucopyranosyl>-β-D-glucopyrnoside

There total 9 articles about 8-azido-3,6-dioxaoctyl 3-O-benzyl-2-deoxy-6-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-gglucopyranosyl>-β-D-glucopyrnoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 106256-80-8
8-azido-3,6-dioxaoctyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

: 4753-07-5
2,3,6,2',3',4',6'-hepta-O-acetyl-lactosyl bromide

: 106256-83-1
8-azido-3,6-dioxaoctyl 3-O-benzyl-2-deoxy-6-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-gglucopyranosyl>-β-D-glucopyrnoside

Guidance literature:: With silver trifluoromethanesulfonate; tetramethylurea; In dichloromethane; -10 deg C, 7 h, RT, 24 h;
DOI:10.1016/0008-6215(86)80016-7

Reference yield:

: 86520-52-7
2-[2-(2-azidoethoxy)ethoxy]ethanol

: 106256-83-1
8-azido-3,6-dioxaoctyl 3-O-benzyl-2-deoxy-6-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-gglucopyranosyl>-β-D-glucopyrnoside

Guidance literature:: Multi-step reaction with 6 steps

1: 90 percent / silver triflate, tetramethylurea / CH₂Cl₂ / 20 h / Ambient temperature

2: 76 percent / M sodium methoxide / methanol / 2 h / Ambient temperature

3: 82 percent / p-toluenesulfonic acid monohydrate / dimethylformamide

4: 95 percent / bariumoxide, barium hydroxide octahydrate / dimethylformamide / 2 h / Ambient temperature

5: 90 percent / 80percent acetic acid / H₂O / 1 h / 80 °C

6: 41 percent / tetramethylurea, silver triflate / CH₂Cl₂ / -10 deg C, 7 h, RT, 24 h

With barium hydroxide octahydrate; sodium methylate; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; acetic acid; tetramethylurea; barium(II) oxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(86)80016-7

Reference yield:

: 77544-68-4
8-tosyloxy-3,6-dioxaoctanol

: 106256-83-1
8-azido-3,6-dioxaoctyl 3-O-benzyl-2-deoxy-6-O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-gglucopyranosyl>-β-D-glucopyrnoside

Guidance literature:: Multi-step reaction with 7 steps

1: sodium azide / dimethylformamide / 2 h / 80 °C

2: 90 percent / silver triflate, tetramethylurea / CH₂Cl₂ / 20 h / Ambient temperature

3: 76 percent / M sodium methoxide / methanol / 2 h / Ambient temperature

4: 82 percent / p-toluenesulfonic acid monohydrate / dimethylformamide

5: 95 percent / bariumoxide, barium hydroxide octahydrate / dimethylformamide / 2 h / Ambient temperature

6: 90 percent / 80percent acetic acid / H₂O / 1 h / 80 °C

7: 41 percent / tetramethylurea, silver triflate / CH₂Cl₂ / -10 deg C, 7 h, RT, 24 h

With sodium azide; barium hydroxide octahydrate; sodium methylate; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; acetic acid; tetramethylurea; barium(II) oxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(86)80016-7