8-azido-3,6-dioxaoctyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:8-azido-3,6-dioxaoctyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:106256-80-8
Molecular Formula:C₂₁H₃₂N₄O₈
Molecular Weight:468.507
Hs Code.:

Synonyms:8-azido-3,6-dioxaoctyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of 8-azido-3,6-dioxaoctyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of 8-azido-3,6-dioxaoctyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 8 articles about 8-azido-3,6-dioxaoctyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 106256-79-5
8-azido-3,6-dioxaoctyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 106256-80-8
8-azido-3,6-dioxaoctyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With acetic acid; In water; at 80 ℃; for 1h;
DOI:10.1016/0008-6215(86)80016-7

Reference yield:

: 86520-52-7
2-[2-(2-azidoethoxy)ethoxy]ethanol

: 106256-80-8
8-azido-3,6-dioxaoctyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / silver triflate, tetramethylurea / CH₂Cl₂ / 20 h / Ambient temperature

2: 76 percent / M sodium methoxide / methanol / 2 h / Ambient temperature

3: 82 percent / p-toluenesulfonic acid monohydrate / dimethylformamide

4: 95 percent / bariumoxide, barium hydroxide octahydrate / dimethylformamide / 2 h / Ambient temperature

5: 90 percent / 80percent acetic acid / H₂O / 1 h / 80 °C

With barium hydroxide octahydrate; sodium methylate; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; acetic acid; tetramethylurea; barium(II) oxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(86)80016-7

Reference yield:

: 77544-68-4
8-tosyloxy-3,6-dioxaoctanol

: 106256-80-8
8-azido-3,6-dioxaoctyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: sodium azide / dimethylformamide / 2 h / 80 °C

2: 90 percent / silver triflate, tetramethylurea / CH₂Cl₂ / 20 h / Ambient temperature

3: 76 percent / M sodium methoxide / methanol / 2 h / Ambient temperature

4: 82 percent / p-toluenesulfonic acid monohydrate / dimethylformamide

5: 95 percent / bariumoxide, barium hydroxide octahydrate / dimethylformamide / 2 h / Ambient temperature

6: 90 percent / 80percent acetic acid / H₂O / 1 h / 80 °C

With sodium azide; barium hydroxide octahydrate; sodium methylate; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; acetic acid; tetramethylurea; barium(II) oxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(86)80016-7