Technology Process of C14H19FN2O3S
There total 3 articles about C14H19FN2O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium on activated charcoal; hydrogen / ethanol / 3361.55 Torr / Inert atmosphere
2: triethylamine / chloroform / 20 °C / Inert atmosphere
With
palladium on activated charcoal; hydrogen; triethylamine;
In
ethanol; chloroform;
DOI:10.1016/j.bmcl.2012.01.045
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 24 h / 0 °C / Inert atmosphere; Reflux
2: triethylamine / chloroform / 20 °C / Inert atmosphere
3: palladium on activated charcoal; hydrogen / ethanol / 3361.55 Torr / Inert atmosphere
4: triethylamine / chloroform / 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; palladium on activated charcoal; hydrogen; triethylamine;
In
tetrahydrofuran; ethanol; chloroform;
DOI:10.1016/j.bmcl.2012.01.045
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 1.5 h / Reflux
2: lithium aluminium tetrahydride / tetrahydrofuran / 24 h / 0 °C / Inert atmosphere; Reflux
3: triethylamine / chloroform / 20 °C / Inert atmosphere
4: palladium on activated charcoal; hydrogen / ethanol / 3361.55 Torr / Inert atmosphere
5: triethylamine / chloroform / 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; palladium on activated charcoal; hydroxylamine hydrochloride; hydrogen; sodium acetate; triethylamine;
In
tetrahydrofuran; ethanol; chloroform; water;
DOI:10.1016/j.bmcl.2012.01.045