C₃₀H₃₉BN₂O₄

Base Information

Chemical Name:C₃₀H₃₉BN₂O₄
CAS No.:1448802-21-8
Molecular Formula:C₃₀H₃₉BN₂O₄
Molecular Weight:502.462
Hs Code.:

C<sub>30</sub>H<sub>39</sub>BN<sub>2</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₃₀H₃₉BN₂O₄

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Technology Process of C₃₀H₃₉BN₂O₄

There total 10 articles about C₃₀H₃₉BN₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1448802-19-4
Cbz-lycodine

: 73183-34-3
bis(pinacol)diborane

: 1448802-21-8
C₃₀H₃₉BN₂O₄

Guidance literature:: With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine; In tetrahydrofuran; at 75 ℃; for 14h; Inert atmosphere;
DOI:10.1002/anie.201208297

Reference yield:

: C₂₄H₂₆N₂O₃

: 1448802-21-8
C₃₀H₃₉BN₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1: Daicel Chiral-Pak AS / ethanol; hexane; diethylamine / Resolution of racemate

2: boron trifluoride diethyl etherate / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

3: triphenylstannane; 2,2'-azobis(isobutyronitrile) / toluene / 0.5 h / 110 °C / Inert atmosphere

4: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine / tetrahydrofuran / 14 h / 75 °C / Inert atmosphere

With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; triphenylstannane; 4,4'-di-tert-butyl-2,2'-bipyridine; In tetrahydrofuran; ethanol; hexane; dichloromethane; diethylamine; toluene; 4: |Miyaura Borylation Reaction;
DOI:10.1002/anie.201208297

Reference yield:

: 1448802-15-0
C₂₄H₂₆N₂O₃

: 1448802-21-8
C₃₀H₃₉BN₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

2: triphenylstannane; 2,2'-azobis(isobutyronitrile) / toluene / 0.5 h / 110 °C / Inert atmosphere

3: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine / tetrahydrofuran / 14 h / 75 °C / Inert atmosphere

With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; triphenylstannane; 4,4'-di-tert-butyl-2,2'-bipyridine; In tetrahydrofuran; dichloromethane; toluene; 3: |Miyaura Borylation Reaction;
DOI:10.1002/anie.201208297