C₃₄H₃₂As₂S

Base Information

Chemical Name:C₃₄H₃₂As₂S
CAS No.:1464833-09-7
Molecular Formula:C₃₄H₃₂As₂S
Molecular Weight:622.537
Hs Code.:

C<sub>34</sub>H<sub>32</sub>As<sub>2</sub>S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₃₂As₂S

Chemical Property:

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Technology Process of C₃₄H₃₂As₂S

There total 2 articles about C₃₄H₃₂As₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 1464833-05-3
2-(tert-butylthio)phenyldiphenylarsine

: 712-48-1
chlorodiphenylarsine

: 1464833-09-7
C₃₄H₃₂As₂S

Guidance literature:: 2-(tert-butylthio)phenyldiphenylarsine; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; at 20 ℃; for 20.75h; Inert atmosphere; Schlenk technique; Cooling with ice;

chlorodiphenylarsine; In hexane; Inert atmosphere; Schlenk technique; Cooling with ice;

With sodium hydroxide; In hexane; water; Inert atmosphere; Schlenk technique;
DOI:10.1071/CH13262

Reference yield:

: 108-98-5
thiophenol

: 1464833-09-7
C₃₄H₃₂As₂S

Guidance literature:: Multi-step reaction with 3 steps

1.1: iron(III) chloride; trichlorophosphate

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexane / 21 h / 10 - 20 °C / Inert atmosphere; Schlenk technique

2.2: 2 h / Inert atmosphere; Schlenk technique

2.3: Inert atmosphere; Schlenk technique

3.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexane / 20.75 h / 20 °C / Inert atmosphere; Schlenk technique; Cooling with ice

3.2: Inert atmosphere; Schlenk technique; Cooling with ice

3.3: Inert atmosphere; Schlenk technique

With iron(III) chloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; trichlorophosphate; In hexane;
DOI:10.1071/CH13262