DL-myo-Inositol 1-Hexadecanoate 4,5-Bis(dihydrogen phosphate) Trimethylammonium Salt (1:2.5)

Base Information

Chemical Name:DL-myo-Inositol 1-Hexadecanoate 4,5-Bis(dihydrogen phosphate) Trimethylammonium Salt (1:2.5)
CAS No.:130277-77-9
Molecular Formula:5C₃H₉N*2C₂₂H₄₄O₁₃P₂
Molecular Weight:1452.62
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of DL-myo-Inositol 1-Hexadecanoate 4,5-Bis(dihydrogen phosphate) Trimethylammonium Salt (1:2.5)

Chemical Property:

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Technology Process of DL-myo-Inositol 1-Hexadecanoate 4,5-Bis(dihydrogen phosphate) Trimethylammonium Salt (1:2.5)

There total 13 articles about DL-myo-Inositol 1-Hexadecanoate 4,5-Bis(dihydrogen phosphate) Trimethylammonium Salt (1:2.5) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87-89-8
D-myo-inositol

: 130277-77-9
DL-myo-Inositol 1-Hexadecanoate 4,5-Bis(dihydrogen phosphate) Trimethylammonium Salt (1:2.5)

Guidance literature:: Multi-step reaction with 13 steps

1: 22.9 percent / TsOH / toluene; dimethylformamide / 2 h / 143 °C

2: 64.5 percent / KOH / 3.5 h / 100 - 125 °C

3: 80.4 percent / 1,2-dihydroxyethane, TsOH / CH₂Cl₂ / 0.78 h / 24 °C

4: NaH / dimethylformamide / 1 h / 25 - 60 °C

5: 1M aq. HCl / ethanol; toluene / 2.5 h / 60 °C

6: 1.) Bu₂SnO / 1.) toluene, 100 deg C, 45 min; 2.) DMF, 95 deg C, 1.5 h

7: 61.6 percent / NaH / dimethylformamide / 2 h / 25 - 40 °C

8: 82 percent / t-BuOK / dimethylsulfoxide / 19 h / 50 °C

9: 83 percent / 1M aq. HCl / ethanol; toluene / 8.5 h / 23 °C

10: 91 percent / pyridine / DMAP / CH₂Cl₂ / 17 h / Ambient temperature

11: 82 percent / DDQ, H₂O / CH₂Cl₂ / 1 h / 25 °C

12: 1.) 1H-tetrazole; 2.) m-chloroperbenzoic acid / 1.) CH₂Cl₂, 25 deg C, 2 h; 2.) 35 deg C, 30 min

13: 1.) hydrogen / 1.) 5percent Pd/C / 1.) EtOH, 1 atm, 25 deg C, 2 h

With pyridine; 1H-tetrazole; hydrogenchloride; potassium hydroxide; potassium tert-butylate; water; hydrogen; sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid; ethylene glycol; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; dmap; palladium on activated charcoal; In ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1002/hlca.19900730428

Reference yield:

: 34361-60-9,55123-24-5,55123-26-7,62012-78-6,104873-71-4
1,2:4,5-dicyclohexylidene-myo-inositol

: 130277-77-9
DL-myo-Inositol 1-Hexadecanoate 4,5-Bis(dihydrogen phosphate) Trimethylammonium Salt (1:2.5)

Guidance literature:: Multi-step reaction with 12 steps

1: 64.5 percent / KOH / 3.5 h / 100 - 125 °C

2: 80.4 percent / 1,2-dihydroxyethane, TsOH / CH₂Cl₂ / 0.78 h / 24 °C

3: NaH / dimethylformamide / 1 h / 25 - 60 °C

4: 1M aq. HCl / ethanol; toluene / 2.5 h / 60 °C

5: 1.) Bu₂SnO / 1.) toluene, 100 deg C, 45 min; 2.) DMF, 95 deg C, 1.5 h

6: 61.6 percent / NaH / dimethylformamide / 2 h / 25 - 40 °C

7: 82 percent / t-BuOK / dimethylsulfoxide / 19 h / 50 °C

8: 83 percent / 1M aq. HCl / ethanol; toluene / 8.5 h / 23 °C

9: 91 percent / pyridine / DMAP / CH₂Cl₂ / 17 h / Ambient temperature

10: 82 percent / DDQ, H₂O / CH₂Cl₂ / 1 h / 25 °C

11: 1.) 1H-tetrazole; 2.) m-chloroperbenzoic acid / 1.) CH₂Cl₂, 25 deg C, 2 h; 2.) 35 deg C, 30 min

12: 1.) hydrogen / 1.) 5percent Pd/C / 1.) EtOH, 1 atm, 25 deg C, 2 h

With pyridine; 1H-tetrazole; hydrogenchloride; potassium hydroxide; potassium tert-butylate; water; hydrogen; sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid; ethylene glycol; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; dmap; palladium on activated charcoal; In ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1002/hlca.19900730428

Reference yield:

: 35949-66-7,58526-04-8,104873-72-5,115509-74-5
(+/-)-1,4-di-O-benzyl-2,3-O-cyclohexylidene-myo-inositol

: 130277-77-9
DL-myo-Inositol 1-Hexadecanoate 4,5-Bis(dihydrogen phosphate) Trimethylammonium Salt (1:2.5)

Guidance literature:: Multi-step reaction with 10 steps

1: NaH / dimethylformamide / 1 h / 25 - 60 °C

2: 1M aq. HCl / ethanol; toluene / 2.5 h / 60 °C

3: 1.) Bu₂SnO / 1.) toluene, 100 deg C, 45 min; 2.) DMF, 95 deg C, 1.5 h

4: 61.6 percent / NaH / dimethylformamide / 2 h / 25 - 40 °C

5: 82 percent / t-BuOK / dimethylsulfoxide / 19 h / 50 °C

6: 83 percent / 1M aq. HCl / ethanol; toluene / 8.5 h / 23 °C

7: 91 percent / pyridine / DMAP / CH₂Cl₂ / 17 h / Ambient temperature

8: 82 percent / DDQ, H₂O / CH₂Cl₂ / 1 h / 25 °C

9: 1.) 1H-tetrazole; 2.) m-chloroperbenzoic acid / 1.) CH₂Cl₂, 25 deg C, 2 h; 2.) 35 deg C, 30 min

10: 1.) hydrogen / 1.) 5percent Pd/C / 1.) EtOH, 1 atm, 25 deg C, 2 h

With pyridine; 1H-tetrazole; hydrogenchloride; potassium tert-butylate; water; hydrogen; sodium hydride; di(n-butyl)tin oxide; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; dmap; palladium on activated charcoal; In ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1002/hlca.19900730428