(CH(CMeNC₆H₃-2,6-(i)Pr₂)2)ZnN(i)Pr₂

Base Information

Chemical Name:(CH(CMeNC₆H₃-2,6-(i)Pr₂)2)ZnN(i)Pr₂
CAS No.:439607-27-9
Molecular Formula:C₃₅H₅₅N₃Zn
Molecular Weight:583.232
Hs Code.:

(CH(CMeNC<sub>6</sub>H<sub>3</sub>-2,6-(i)Pr<sub>2</sub>)2)ZnN(i)Pr<sub>2</sub>

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Chemical Property of (CH(CMeNC₆H₃-2,6-(i)Pr₂)2)ZnN(i)Pr₂

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Technology Process of (CH(CMeNC₆H₃-2,6-(i)Pr₂)2)ZnN(i)Pr₂

There total 1 articles about (CH(CMeNC₆H₃-2,6-(i)Pr₂)2)ZnN(i)Pr₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 210832-39-6
N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine

: 7646-85-7,24359-56-6
zinc(II) chloride

: 4111-54-0
lithium diisopropyl amide

: 439607-27-9
(CH(CMeNC₆H₃-2,6-(i)Pr₂)2)ZnN(i)Pr₂

Guidance literature:: In tetrahydrofuran; under N2 atm. THF was added to mixt. ligand and LiN(i)Pr2, stirred for 30 min and added to soln. ZnCl2 in THF, soln. was stirred for 1 h; solvent was removed in vacuo, residue was extd. with hexane;
DOI:10.1021/ic020148e

Reference yield: 99.0%

: 439607-27-9
(CH(CMeNC₆H₃-2,6-(i)Pr₂)2)ZnN(i)Pr₂

: 124-38-9,18923-20-1
carbon dioxide

: 439607-32-6
(CH(CMeNC6H3-2,6-(i)Pr2)2)Zn(η2-O2CN(i)Pr2)

Guidance literature:: In benzene; CO2 was bubbled through soln. Zn complex in benzene for 10 min; solvent was removed; elem. anal.;
DOI:10.1021/ic020148e

Reference yield: 92.0%

: 439607-27-9
(CH(CMeNC₆H₃-2,6-(i)Pr₂)2)ZnN(i)Pr₂

: 75-65-0
tert-butyl alcohol

: 439607-28-0
(CH(CMeNC₆H₃-2,6-(i)Pr₂)2)ZnO(t)Bu

Guidance literature:: In toluene; under N2 atm. to soln. Zn complex in toluene at -78°C soln. t-BuOH in toluene was added dropwise, mixt. was allowed to warm slowly to room temp. and stirred for 15 min; volatiles were removed in vacuo; elem. anal.;
DOI:10.1021/ic020148e