3-chloro-2-phenylselenobutyl acetate

Base Information

• Chemical Name: 3-chloro-2-phenylselenobutyl acetate
• CAS No.: 80663-63-4
• Molecular Formula: C₁₂H₁₅ClO₂Se
• Molecular Weight: 305.663

Synonyms:

Chemical Property of 3-chloro-2-phenylselenobutyl acetate

Chemical Property:

Purity/Quality:

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Technology Process of 3-chloro-2-phenylselenobutyl acetate

There total 3 articles about 3-chloro-2-phenylselenobutyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Phenylselenyl chloride (5707-04-0) + trans-2-butenyl acetate (7204-29-7) → 3-chloro-2-phenylselenobutyl acetate (80663-63-4) + 2-chloro-3-phenylselenobutyl acetate

Guidance literature:

In chloroform; at 25 ℃;

DOI:10.1021/jo00346a022

Reference yield:

Phenylselenyl chloride (5707-04-0) + trans-2-butenyl acetate (7204-29-7) → 3-chloro-2-phenylselenobutyl acetate (80663-63-4) + Acetic acid 2-chloro-1-pentyl-3-phenylselanyl-hexyl ester

Guidance literature:

In chloroform; at 25 ℃;

DOI:10.1021/jo00346a022

Reference yield:

Phenylselenyl chloride (5707-04-0) + crotyl acetate (628-08-0) → 3-chloro-2-phenylselenobutyl acetate (80663-63-4) + 2-chloro-3-phenylselenobutyl acetate

Guidance literature:

With zinc(II) chloride; In chloroform-d1; Title compound not separated from byproducts;

DOI:10.1016/j.tet.2004.05.084

upstream raw materials:

Phenylselenyl chloride

trans-2-butenyl acetate

crotyl acetate

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