diphenylstyrylphosphine borane

Base Information

Chemical Name:diphenylstyrylphosphine borane
CAS No.:1256268-29-7
Molecular Formula:C₂₀H₂₀BP
Molecular Weight:302.164
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenylstyrylphosphine borane

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Technology Process of diphenylstyrylphosphine borane

There total 1 articles about diphenylstyrylphosphine borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 1.0%

: 139286-41-2
(S)-tert-butyl 2-phenylethylsulfoxide

: 13292-87-0
dimethyl sulfide borane

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1256268-29-7
diphenylstyrylphosphine borane

: ((CH₃)3CSOCH(CH₂C₆H₅)P(C₆H₅)2)BH₃

Guidance literature:: With methyllithium; In tetrahydrofuran; diethyl ether; (N2); addn. of ethereal soln. of methyllithium to THF soln. of sulfoxidederiv. at -78°C, keeping for 0.5 h, addn. of phosphine deriv. in THF at -78°C, keeping for 30 min, addn. of boron compd., slow wa rming to room temp. for 3 h; addn. of water, extn. (ethyl acetate), chromy. (silica gel, hexane/ethylacetate (10:1));
DOI:10.1021/om900438v