1-bromo-3-(methoxymethoxy)-2-methyl-4-phytylbenzene

Base Information

Chemical Name:1-bromo-3-(methoxymethoxy)-2-methyl-4-phytylbenzene
CAS No.:149982-00-3
Molecular Formula:C₂₉H₄₉BrO₂
Molecular Weight:509.611
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-bromo-3-(methoxymethoxy)-2-methyl-4-phytylbenzene

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Technology Process of 1-bromo-3-(methoxymethoxy)-2-methyl-4-phytylbenzene

There total 2 articles about 1-bromo-3-(methoxymethoxy)-2-methyl-4-phytylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7766-23-6
3-bromo-2-methylphenol

: 149982-00-3
1-bromo-3-(methoxymethoxy)-2-methyl-4-phytylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / (i-Pr)2NEt / CH₂Cl₂; methyl acetate / 1 h / Ambient temperature

2: 1.) PhLi, 2.) CuBr / 1.) Et₂O, reflux, 7 h, 2.) EtO₂, r.t., overnight

With phenyllithium; N-ethyl-N,N-diisopropylamine; copper(I) bromide; In dichloromethane; acetic acid methyl ester;
DOI:10.1002/hlca.19930760429

Reference yield:

: 4444-13-7
phytyl bromide

: 149981-99-7
1-Bromo-3-(methoxymethoxy)-2-methylbenzene

: 149982-00-3
1-bromo-3-(methoxymethoxy)-2-methyl-4-phytylbenzene

Guidance literature:: With phenyllithium; copper(I) bromide; Yield given. Multistep reaction; 1.) Et₂O, reflux, 7 h, 2.) EtO₂, r.t., overnight;
DOI:10.1002/hlca.19930760429

Reference yield:

: 149982-00-3
1-bromo-3-(methoxymethoxy)-2-methyl-4-phytylbenzene

: 149982-08-1
2,3-Dimethyl-6-phytylphenol

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) tetramethylethylenediamine, BuLi / 1.) Et₂O, hexane, 0 deg C, 1 h, 2.) -25 deg C, 5 min

2: 57 percent / diethyl ether

3: 93 percent / LiAlH₄ / diethyl ether / 1 h / 0 °C

4: 64 percent / LiAlH₄, titanocene dichloride / tetrahydrofuran / 2.5 h / Heating

With lithium aluminium tetrahydride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; titanocene dichloride; In tetrahydrofuran; diethyl ether;
DOI:10.1002/hlca.19930760429