N-(2-bromophenyl)-2-thiophenecarboxamide

Base Information

Chemical Name:N-(2-bromophenyl)-2-thiophenecarboxamide
CAS No.:136340-96-0
Molecular Formula:C11H8BrNOS
Molecular Weight:282.161
Hs Code.:
Mol file:136340-96-0.mol

Synonyms:thiophene-2-carboxylic acid 2-bromoanilide;Thiophene-2-carboxylic acid (2-bromo-phenyl)-amide;N-(2-bromophenyl)thiophene-2-carboxamide;

Suppliers and Price of N-(2-bromophenyl)-2-thiophenecarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-bromophenyl)-2-thiophenecarboxamide

Chemical Property:

Melting Point:115 - 117 °C
PSA：57.34000
LogP:3.83590

Purity/Quality:

Safty Information:

Pictogram(s):
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Technology Process of N-(2-bromophenyl)-2-thiophenecarboxamide

There total 3 articles about N-(2-bromophenyl)-2-thiophenecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 5271-67-0
2-Thiophenecarbonyl chloride

: 615-36-1
2-bromoaniline

: 136340-96-0
thiophene-2-carboxylic acid (2-bromophenyl)amide

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1016/j.tet.2007.08.013

Reference yield: 88.0%

: 3437-95-4,149762-92-5
2-Iodothiophene

: 201230-82-2
carbon monoxide

: 615-36-1
2-bromoaniline

: 136340-96-0
thiophene-2-carboxylic acid (2-bromophenyl)amide

Guidance literature:: 2-Iodothiophene; 2-bromoaniline; With palladium diacetate; triethylamine; In water; for 0.166667h;

carbon monoxide; In water; at 100 ℃; for 8h; under 10343.2 Torr;
DOI:10.1080/00397911.2010.523155

Reference yield:

: 527-72-0
2-thiophenylcarboxylic acid

: 136340-96-0
thiophene-2-carboxylic acid (2-bromophenyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 1 h / Heating

2: toluene

With thionyl chloride; In toluene;